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GC/MS analysis results for sample AD23606, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23606 conducted on October 19, 2001.

NYC-WTC_000088961–000088985

Folder label: “GC/MS Scan 9/27/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23606.D Vial: 13 Acq On : 17 Oct 2001 1:59 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method ; C;\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 12 Octadecane Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 33.69 2.36 ug/1 284871 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 91 2 Heneicosane 296 C21H44 000629-94-7 91 3 Tetracosane 338 C24H50 000646-31-1 91 4 Pentacosane ____________________ 352 C25H52 000629-99-2 91 Abundance Scan 3121 (33.693 min): 23606.D (-) m/z 57700 100.00% ' 57

43 71

5000- 85

LL iH—i—r=f 33.40 33.60 33.80 34.00 m/z71.10 72.26% tn/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Octadecane 57 43 71

85 5000 ..... , ,Si...... 33.40 '33.60' 'so^SO 34'00 QQ m/z 43705 68.43% 224 254 '' I' ‘ I '' ' ' I' ' ' ' I I'' ’' I' *'' I ni/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #42201; Heneicosane .5|7 71 ' I ' ' '' ' ‘ I ' ' 33.40 33.60 33.80 34.00 85 5000 m/z 85.05 49.58% 99 fl pAO,I ^]A^141155 268 296

A I ' '"I I I • I I 1 I . . . I I H I J . . I • I • H I I . . . . I " I ’" ’ I' mZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane ' ' I ' ' 43 57 . 33.40 33.60 33.80-34.00 _ 71 m/z 417.05-’--^ 24.82%

5000 85 fl 99 I p-rrqpI l| 155169183197 294 I' " ' I " ' • I'''' I 338 p'' 'I ’ 'n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 33.40 33.60 33.80 34.00

23606.D NP091101.M Thu Oct 18 10:36:04 2001 Page 12

NYC-WTC_000088979

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NYC-WTC_000088979Source: NYC Law Department, mirrored locally

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