GC/MS analysis results for sample AD23650, Oct 2001

NYC 9/11 Public Portal Document

Library Search_Compound_Report

Data File : C:\HPCHEM\1\DATA\OCT1601\23650.D Vial: 15 Acq On : 17 Oct 2001 3:56 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 - MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 11 Tetracosane Concentration Rank 4

R.T. EstConc Area 'Relative to ISTD R.T.

32.73 1.35 ug/1 163992 Chrysene-dl2 33.13

Hit# of 5 Tentative ID MW MolForm CAS# Qual \

1 Tetracosane 338 C24H50 000646-31-1 9 2 Pentacosane 352 C25H52 000629-99-2 9 3 Octadecane 254 C18H38 000593-45-3 87 4 Heneicosane 296.C21H44 000629-94-7.87 Abundance Scan 3016 (32.732 min): 23650.D (-) m/z 57.00 100.00% 57 43 71 85 5000

T rrr . I'l .T, ■ , I.. . 32.40 32.60 32.80 33.00 m/z TITTo 72.94% •nlz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71 / 5000 85 I ' ' ' I 32.40 32.60 32.80 33.00 m/z 43705 70777% ,. L jL .'L.M ........ .... A Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance------ --- .— . -#73718: Pentacosane—--- ------ ------- 4(3 5|7 T-5=7-rT-r-r-p--A-T^f=r^^ 32.40 32.60 32.80 33.00 71 5000 m/z 85.05 52.31% 85 I ■nZz-> 40 60 , A 80,J, .T,100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71560: Octadecane . _ 43 5(7. 32.40 32.60 -32 80-33.00 m/z 41.05 28.28% 71 253 85

99 ■, I ■ ■ ■'J, ■ J, ...................... ■n/z-> 40 60 80 'lOO 120 'l4o' 'l6o' 'l80 200 '^0 2^' 260 280'3Oo' 320 340 32.40 32.60 32.80 33.00

23650.D NP091101.M Thu Oct 18 10:40:26 2001 Page 11;

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