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GC/MS analysis results for sample AD23650, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23650 conducted on October 19, 2001.

NYC-WTC_000089000–000089024

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000089016
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NYC 9/11 Public Portal Document

LibrarY_Sear.ch,..Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23650.D Vial: 15 Acq On : 17 Oct 2001 3:56 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L

Peak Number 10 Hexatriacontane Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.74 1.39 ug/1 168577 Chrysene-dl2 33.13

Hit# of 5 Tentative ID MW MolForm CAS# Qual (jj Hexatriacontane 507 C36H74. 000630-06-8 9:^ 2'' Tetracosane 338 C24H50 000646-31-1 90 3 Pentacosane 352 C25H52 000629-99-2 87 4 Octadecane 254 C18H38 000593-45-3 87 Abundance Scan 2908 (31,741 min): 23650,D (-) m7z SYTOO 100.00% 57

43 71

5518! 85

99 .. /V.l ' I ' ' ' ' I 31,40 31,60 31,80 32,00 m/z 71705 70.85% Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #74636: Hexatriacontane 43 57

5000 71 85 a 31,40 31,60 31,80 32.00 m/z 4^705 66.58% I T ^J3127141 155169183197211 . . . I , , T , I 11 , , I' 1 1 11 I I 11 I I I , I , I I I I 1 I''' ’ I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance—------ - ‘#73543;-Tetracosane------- ------ ----- 43 5t7 71

85 M 31.40 31.60 31.80 32.00 m/z 85.05 48.52% 553

99 l| '’P’'27 1551691^197 ' 294 338 I ' I' ''' I'' ‘' I'' I''''' I '''' I'''' I'''' I'''' i'' '' r ''' I n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance__ _ #73718:,Pentacosane_ . Al 43 5,7;^^^ —31,40 31,60 31.80 - 32.00- “m/z 41700 26735% 71 5000

JU - -85

I .J...- 113127141155169183197211225 1 I . I . I I I I . I l' I I I 'i I I . . . I I I . . I I . t I I rn- r I' ’'' I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23650.D NP091101.M Thu Oct 18 10:40:24 2001 Page 10

NYC-WTC_000089016

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NYC-WTC_000089016Source: NYC Law Department, mirrored locally

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