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GC/MS analysis results for sample AD23650, Oct 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23650 conducted on October 19, 2001.

NYC-WTC_000089000–000089024

Folder label: “GC/MS Scan 9/27/01

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Scanned page image, NYC-WTC_000089015
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1601\23650.D Vial: 15 Acq On - : 17 Oct 2001 3:56 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) .Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Octadecanoic acid, 2-methylpro Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 31.65 0.84 ug/ 102147 Chrysene-dl2 33.13 Hit# of 5 fentative ID MW MolFprm ■ CAS# Qual

1 Octadeca: ic acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 70 2 Butyl t»>tradecanoate (myristate) 284 C18H36O2 000000-00-0 58. 3 Octade^:noic acid, butyl ester 340 C22H4402' 000123-95-5 42 4 Oxira/fe, 2,3-bis (1-methylethyl)-, t 128 C8H16O 054644-32-5 32 Abundance Scan 2898 (31.649 min): 23650.D (-) 56.00 100.00%

552 4' 73 129 285 ill r . .143157171 227241 1 ^40 31.40 31.60 31.80 32.00 I n 1’“ t I T'l I I I T I i' I I I I 'i I I i' I I I i I j I I I I I I I I I I I I I I I I I I I I I I I I rI I I I I I I 1 I I I I I I I I m/z 57.00 . 56737% nZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 57

5000 31.40 31.60 31.80 32.00 285 m/z 43705 39.94% 267 J T i.7inT 1111II111111 r111 i 11 185 I''' ' I • • ‘ • I ' 1 ' • I rI I I I 340

n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance -------------------------- #40186: Butyl tetradecanoate (myristate)------ " 53

31.40 31.60 31.80 32.00 5000 m/z 41.05 35.08% 229 211 284 ' J ‘' I' ‘ ' I'''' I I' ‘ ‘' r ''' Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance ___ #73570:.0ctadecanoic acid, butyl ester. T f7ii I -I /y4- 53 : - 31-.4O-31:60' 31.80 32.00 m7z 55700 31777% ___ 5000 ------285 340.

■n/z-> 40 uxXttX 60 73 129

TfVTT*^hn-VfTT-T*-rTY 185 I 241 I' ''' I'''' I ‘' I'''' I'''' I'''' I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 I 267

p-rrry . " I " . ■ ................... ......................... 31.40 31.60 31.80 32.00

23650.D NP091101.M Thu Oct 18 10:40:22 2001 Page 9

NYC-WTC_000089015

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NYC-WTC_000089015Source: NYC Law Department, mirrored locally

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