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GC/MS analysis results for sample AD22977, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22977 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087731–000087753

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0301\22977.D Vial: 3 Acq On 3 Oct 2001 2:36 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L it******************************************************************** Peak Number 8 Tetracosane Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.76 1.03 ug/1 141717 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 9K 2 Octadecane 254 C18H38 000593-45-3 91 ^ 3 Pentacosane 352 C25H52 000629-99-2 91 / 4 Heptadecane 240 C17H36 000629-78-7 90/ Abundance Scan 2911 (31.761 min): 22977.D (-) m/z 57.00 100.00% 57 71 43 85 5000

m/z-> Abundance 40 w 60 T* 80 T 155169183197 100 120 140 160 180 200 220 240 260 280 300 320 340 #73543: Tetracosane T ...... .P.Pv..... . 31.40 31.60 31.80 32.00 m/z 71.00 73.29%

43 5 7 71

5000 85 31.40 31.60 31.80 32.00 99 m/z 43.00 66.54% l| \|3''27 155169183197 i j I, T^Y^rTTH-pVrryTTTVp-r'Tn-p-T-TT^ 294 I . I ■ . I . 11 . I . . ,Ty 338 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71560: Octadecane 43 57

71 31.40 31.60 31.80 32.00 5000 85 m/z 85.05 50.18% 99 t 1 1 ,j 169183197 254 -rp-n-q-r ‘ ' I ' ' ‘ ' 1 ' ' ' ' I ' ''' I ' ' ‘ ' 1 ' ' ‘ ' p-m-p-TT-rj jn/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 (Abundance #73718: Pentacosane 4(3 5,7 31.40 31.60 31.80 32.00 m/z 41.05 25.30% 71 A mil 85

I, ''Pl27l41155169183197211225 ' ' I ''' ' I ' ' ' ' I ' ' ' I ' ' ' ' I ' ' ' ' ’ ' I ' •' ■p m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

22977.D NP091101.M Tue Oct 09 09:48:43 2001 Page 8

NYC-WTC_000087745

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NYC-WTC_000087745Source: NYC Law Department, mirrored locally

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