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GC/MS analysis results for sample AD23260, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23260 conducted on October 12, 2001.

NYC-WTC_000088079–000088097

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088091
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT0901\23260.D Vial: 6 Acq On :. 9 Oct 2001 6:15 pm Operator: 209 GALOS Sample : g c/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DAT7kBASE\NBS75K.L ********************************************************************* Peak Number 6 Tetracosane Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 32.74 1.04 ug/1 198876 Chrysene-dl2 33.13 Hit# of 5 Tentative ID MW MolFom CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 91, 2 Heptadecane, 9-octyl- 352 C25H52 007225-64-1 91 3 Heptadecane 240 C17H36 000629-78-7 91 4 Pentadecane 212 C15H32 000629-62-9 86 Abundance Scan 3017 (32.737 min): 23260.D (-) m/z SYTOO 100.00% 5|7 ■

85 Sia 4

TiZz-> \bundance 40 4xH 169 197 225 281 ' 1 ’'" I " " I " " I " " I' " ' I " " I " " I " ' ’ I' " ' I " " I 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #73543: Tetracosane 32,40 32,60 32,80 33,00 m/z 71.00 (1 76722%

57

253 85 Ik 32,40 32.60 32.60 33,00 m/z43705 69.79% J J ll T . 183 294 11 n I I'T 111111V111iTp 11111 r.. I "i 11 .■ I 338 ' 'I'''' I I'''' I -n/2-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ^bundance #49558: Heptadecane, 9-octyl- 57

T 32,40 32,60 32,80 33,00 5000 85 m/z 85.05 53.86%

239 310 352 p-n-rj- I' ' p' ' ’I•'''I‘ ‘ * 1' ' ' ' I ' ' '' I 1’' I tVz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance 57 #71193: Heptadecane i, 32,40 32,60 32,80 33,00 m/z 41705 25753%

5000 85

210 240 I " ‘' I' ‘' I' ‘ I ‘' I''' ‘ I'''' I''' ‘ I Tlfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32,40 32,60 32,80 33,00

23260.D NP091101.M Thu Oct 11 10:44:00 2001 Page 6

NYC-WTC_000088091

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NYC-WTC_000088091Source: NYC Law Department, mirrored locally

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