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GC/MS analysis results for sample AD23081, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23081 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087842–000087862

Folder label: “GC/MS Scan 9/21/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT0301\23081.D Vial: 8 Acq On : 3 Oct 2001 7:29 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Tetracosane Concentration Rank 10

R.T. EstConc Area Relative to ISTD R.T.

30.72 0.55 ug/1 81456 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Tetracosane 338 C24H50 000646-31-1 91, 2 Pentacosane 352 C25H52 000629-99-2 91 3 Heptadecane, 2,6,10,15-tetramethyl- 296 C21H44 054833-48-6 90 4 Docosane 310 C22H46 _______ 000629-97-0 86 Abundance Scan 2798 (30.724 min): 23081 .D (-) m/z 57.00 100.00% 57 71 43 85 5000

30.40 30.60 30.80 31.00 ...................... m/z 71.10 74.29% LAbundance 60 80 100 120 140 1 60 180 200 220 240 260 280 300 320 340 #73543: Tetracosane 43 57 71 \ -rj- 5000 I 30.40 30.60 30.80 31.00 ! 99 m/z 43.05 67.77% j,i |l \Pl27 155169183197 I I '' i '' 5 ' ' 294 338 m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 'Abundance #73718: Pentacosane 43 57

71 30.40 30.60 30.80 31.00 5000 85 m/z 85.05 52.53%

113127141155169183197211225 I''' ‘ I'''' I m/z--> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 _320_340 Abundance " #42196: Heptadecane, 2.6,10,15-tetramethyl- T 30.40 30.60 30.80 31.00 71 m/z 41.05 28.15% 85

T 183 211 268 296 ' I ' ' " ' I ' ' ' ' i ' ' ' I . . . I I '■ ■ ■ ■ I ■ ■ ■ ■ I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 30.40 30.60 30.80 31.00

23081.D NP091101.M Tue Oct 09 10:05:10 2001 Page 4

NYC-WTC_000087852

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NYC-WTC_000087852Source: NYC Law Department, mirrored locally

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