GC/MS analysis report for sample AD22494, September 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2501\22494.D Vial: 5 Acq On : 25 Sep 2001 6:21 pm Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 Octadecane Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

32.76 3.10 ug/1 352148 •Chrysene-dl2 33.15

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Octadecane 254 C18H38 000593-45-3 91 2 Eicosane 282 C20H42 000112-95-8 91 3 Pentacosane 352 C25H52 000629-99-2 91 4 Tetracosane 338 C24H50 000646-31-1 91 AifcHindance Scan 3020 (32.763 min): 22494. D (-) m/z 57700 100.00% 57

85 5000 4- J 1 J i i J . 1?7 225 253 281 ... n..... . 32.40 32.60 32.80 33.00 352 m/z 71.00 757'01% T™7 rTpTfTj IT I I i" I I p I iTi I n I I p ■« n I I r I I p । । r। m i । r । । । p । r । । । । । । । । । I '' ' ' I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #71561: Ocfadecane 57

5000 85 / y 32.40 32.60 32.80 33.00 m/z 43.05 68.64% -rrp- p-m-p-n-rp 224 ^ . I . . r.-pn-t". I p-rTp-rTTpTT-rp-rT-rry A 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340

A \bundance #39862: Eicosane 57

32.40 32.60 32.80 33.00 5000 85 m/z 85.05 52.76% I , ■ A ■ ,L. A, Jh J fl.'........1??................ ............... m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 r-pTT-TT-pTT-Zp-T-r-rT-p-r-f^^ Abundance #73718: Pentacosane 43 32.40 32.60 32.80 33.00 m/z 41705 25.55% 71 A 5000

,...... ............ -rp-n-rp- I I . IT. . I I . . I I I I i-i I I . I I I [ . I I . I . I . I I . I I I I I " ' ' I " " I ' " ’ I * ' ' ' I ' ' ’ • I ' " ' I m/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 32.40 32.60 32.80 33.00

22494.D NP091101.M Wed Sep 26 15:26:48 2001 Page 4 NYC-WTC_000086857