GC/MS analysis report for sample AD22494, September 2001

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2501\22494.D Vial: 5 Acq On : 25 Sep 2001 6:21 pm Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Tetracosane Concentration Rank 6

R.T. EstConc Area Relative to ISTD R.T.

31.77 3.00 ug/1 340734 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qua! (^^'Tetracosane 338 C24H50 000646-31-1 99 2 Hexadecane 226 C16H34 000544-76-3 91 3 Heneicosane 296 C21H44 000629-94-7 91 4 Heptadecane 240 C17H36 000629-78-7 91 Abundance Scan 2912 (31.771 min): 22494.D (-) m/z 57700 170770%

43 71

5000 85

' I ' ‘ ‘ ' I JU... T I I ITl I I I • » I I r I, i i hl \r‘'?^''^''1^169l83197211225239253267281 31 40 31.60 31.80 32.00 32.20 338 m/z 71.00 7/790% 0 । ■ ■ ■ ■ । ■ ■ ■ > । ■ T| I n I jTI. q I iTi I n ) . f 11 i'i 11 r 111'l I I r 111'l i । r i i i) । '' I'''' I'' Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73543: Tetracosane 43 57 71

5000 85 31.40 31.60 31.80 32.00 32.20 m/z 43.05 63.33% -r-rp-r in ,,, A, J.. ii, ■ .'17.^.. ........... ...... ■ (1 'n^-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #29267: Hexadecane T 71 31 40 31.60 31.80 32.00 32.20 5000- 85 m/z 8^700^ 48.97%

99

Ti/z-> 40 60 4 100J •prrr^Tr P i । A i i |' i i 80 196 226 120 140 160 180 200 220 240 260 280 300 320 340 Abundance 57 #42201: Heneicosane . . A.H ..... 31 40 31.60 31.80 32.00 32.20 71 in/z 41705 25.11% 85 5000

99

■nfe-> 44 • V ' “ • I ' • • • I ' • •' I 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 p-TT-ry 268 296 31.40 31.60 31.80 32.00 32.20

22494.D NP091101.M Wed Sep 26 15:26:46 2001 Page 3 NYC-WTC_000086856