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GC/MS analysis report for sample AD22494, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22494 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086852–000086871

Folder label: “508 Scan 9/15/01 9/26/01

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Scanned page image, NYC-WTC_000086855
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2501\22494.D Vial: 5 Acq On : 25 Sep 2001 6:21 pm Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 Butyl tetradecanoate (myristat Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T.

31.67 3.38 ug/1 385013 Chrysene-dl2 ,33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

lutyl tetradecanoate (myristate) 284kC18fl36O2! 000000-00-0 86 ^-zoctadecanoic acid, 2-methylpropyl e 340 C22H44O2i 000646-13-9 38 3 Cyclopropane, 1-(1-methylethyl)-2-n 210 C15H30 041977-39-3 35 4 2-Decene, 9-methyl-, (Z) -___________ 154 C11H22 074630-24-3 25 Abundance Scan 2901 (31.670 min): 22494.D (-) Tm/z 56.00 100.00% 55

5000 4 73 129 285 h J .'.^I Tl V.! I., 5^157171^^1^ .227241 [ 31.40 31.60 31.80 32.00 T-rp-T I f. 1 T I I f l I I ri I T I I 1 tT I 'i' I I I I 'i, I I I I I I I I ,1 I I I I , I , I I > I I I , I I I I 11 I I I r, I I I > I I > I I m/z SYTOO 50.40% TT/z-> Abundance 40

53 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 #40186: Butyl tetradecanoate (myristate) fl 5000 229 31.40 31.60 31.80 32.00 211 m/z 43.05 427^7%

Tlfe-> Abundance 40 -n-p-r U&x 60 p-TT-rph-TTyrr^rrp-fhn^^ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 284 ' J ''' I'''' I'''' I #48214; Octadecanoic acid, 2-methylpropyl ester 5(7

31.40 31.60 31.80 32.00 5000 m/z 41.00 31.29% 285 267 J 1^ 241 [ I 340 , I I , I', I , . , Fl I I-U I I'' ‘' I'''' I''' * 1''' ‘ * I' ' I ' I Tife-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #25482; Cyclopropane, 1 -(1 -methylethyl)-2-nonyl- 55 31.40 31.60 31.80 32.00 m/z 28.70%

5000

70 42 ^1^125 1^ 182 210 / I'''' I T T ■p" mfe-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

22494.D NP091101.M Wed Sep 26 15:26:44 2001 Page 2 NYC-WTC_000086855

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NYC-WTC_000086855Source: NYC Law Department, mirrored locally

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