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GC/MS analysis results for sample AD23270, Oct 15 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23270 conducted on October 15, 2001.

NYC-WTC_000088346–000088371

Folder label: “GC/MS Scan 9/25/01

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Scanned page image, NYC-WTC_000088361
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File': C:\HPCHEM\1\DATA\OCT1201\23270.D vial: 18 Acq On : 12 Oct 2001 6:44 pm Operator: 209 • GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 9 Butyl tetradecanoate (myristat Concentration Rank 7 R.T. EstConc Area Relative to ISTD R.T. 31.64 2.06 ug/1 218857 Chrysene-dl2 33.12 Hit# of 5 Tentative ID MW MolForm CAS# Qual Butyl tetradecanoate (myristate) 284 C18H36O2: 000000-00-0 86 Z Octadecanoic acid, butyl ester 340 C22H44O2i 000123-95-5 64 3 Cyclobutane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 38 4 Cyclopropane, 1-(1-methylethyl)-2-n 210 C15H30 041977-39-3 38 Abundance Scan 2897 (31.639 min): 23270.D (-) m/z 56.00 100.00% 50

5000 4' 73 129 285 I ' ' ' ' I 31,40 31.60 31,80 32.00 ,, J I I III I > I ’ll 1 I ' ' ■ 340 I > I I > I I I ■ I I ■ I I I > I • ■ I ■ ' I I I I I I j I T I I I ■ I • I I I I I I I I I I m/z 5^7700 49.04% ii/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 53

5000 229 31.40 31.60 31.80 32.00 73 m/z 43705 40.27%

u.,0X1 129 211

I'' " I'' ' I'' ‘' I''" I"'' I'"' I' Tl/Z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester 50 TT-p-r 31.40 31.60 31,80 32.00 55a m/z 41.05 35.91% 285 340 73 129 267 185 I' " ' I'' I I'''' I'''' I'''' I Y I I 'f " " I' ' ‘I '' I " " I ■Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #21985: Cyclobutane, 1,1-dimethyl-2octyl- 5 31.40 31.60 31.80 32.00 m/z 73.00 31.60%

55a

27 I ( , 111 140 168 196 I'' " I' ‘ pTVrTtTT-^lTTrVTyrTTTlTTrTTp+TTpTTTJTTT^^ ''I' 'I'‘ 'I'' TTfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

23270.D NP091101.M Mon Oct 15 09:33:46 2001 Page 9

NYC-WTC_600d88361

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NYC-WTC_000088361Source: NYC Law Department, mirrored locally

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