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GC/MS analysis report for sample AD22493, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22493 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086827–000086851

Folder label: “508 Scan 9/15/01 9/26/01

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Scanned page image, NYC-WTC_000086837
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2501\22493 .D Vial: 4 Acq On : 25 Sep 2001 5:22 pm Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 Butyl tetradecanoate (myristat Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T.

31.68 4.51 ug/1 530754 Chrysene-dl2 33.15

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Butyl tetradecanoate (myristate) 284 C18H36O2 000000-00-0 64 Octadecanoic acid, 2-methylpropyl e 340 C22H44O2 000646-13-9 64 3 Octadecanoic acid, butyl ester 340 C22H44O2 000123-95-5 45 4 Cyclobutane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 Abundance Scan 2901 (31.677 min): 22493.D (-) m/z 56.00 100.00% 53

5000 4- 73 129 285

Ti/z-> XIMUW 40 60 80 143157171199213227241 100 120 140 160 180 200 220 240 260 280 300 320 340 340 _3t4g_3t^_3r8g_32;00_ m/z 57.00 51.46% (Vbandance #40186: Butyl tetradecanoate (myristate) 55

5000 229 ‘ ' I ' ' ' ' I 31.40 31.60 31.80 32.00 1 T

211 m/z 43.05 39.06% 284 I... I'''' I'''' I'''' I' I I'''' J ''' I'''' I'''' I ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 /Abundance #48214: Octadecanoic acid, 2-methylpropyl ester 57

31.40 31.60 31.80 32.00 5000 m/z 41.00 34.56%

267 285 J fl 4 241 [ I 340 . ,, 1.111 I... r I .... I I'''' I'''' I'''' 1'''' I'''' I 'I Ti/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #73570: Octadecanoic acid, butyl ester I ’ ' ' ‘ I ' ' ' ' I 5|B 31.40 31.60 31.80 32.00 m/z 73700 317^3% 5000 285 340

40 u 60 73 129 185 I I ‘' r ' ‘' I ’r I 267

• I'''' I'''' r ' • 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

22493.D NP091101.M Wed Sep 26 11:36:41 2001 Page 3

NYC-WTC_000086837

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NYC-WTC_000086837Source: NYC Law Department, mirrored locally

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