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GC/MS analysis results for sample AD23125, Oct 2001

Machine-extracted title · confidence 90%

Laboratory report documenting GC/MS analysis of sample AD23125 conducted on October 12, 2001.

NYC-WTC_000088023–000088043

Folder label: “GC/MS Scan 9/24/01

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Scanned page image, NYC-WTC_000088035
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NYC 9/11 Public Portal Document

Library Search Compound' Report

Data File C:\HPCHEM\1\DATA\OCT0401\23125.D Vial: 13 Acq On 5 Oct 2001 3:16 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise 1 -Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : iC:\HPCHEM\1\METHODS\NP091101. M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Butyl tetradecanoate (myristat Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

31.66 1.64 ug/1 323413 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

Butyl tetradecanoate (myristate) 284 C18H36O2 000000-00-0 86 2^Octadecanoic acid, butyl ester 340 C22H44O2 000123-95-5 40 3 Cyclobutane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 35 4 Pentadecane, 8-methylene- 224 C16H32 055668-09-2 32 Abundance ~ , Scan 2900 (31.663 min): 23125.D (-) m/z 56.0,0 100.00% £5 fl

5000 4 73 129 285 I ■ T 340 31.40 31.60 31.80 32.00 [T I I rf I 111 jn I I ~| I I t TI I I I *1 I *1 I I I I I I I I I I I I I T~i I I I I I I I I I I ( I I 11 b I I "i I I I rTfr. m/z 57.00 52.90% im/z~> 20 40 60 80 100 '120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 56 I

5000 229 31.40 31.60 31.80 32.00

Ju 73 I 211 m/z 43.05 40.96% 129 284 I p^TTTp-rVTqT-tVrprrTT-y ■ 11' • ’ I" " I' ’'' I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 'Abundance #73570; Octadecarioic acid, butyl ester 56 ............ 31.40 31.60 31.80 32.00 5000 285 m/z 35.95% 340 73 129 267 ■! 185 241 ' 'I' ' ' 'I' ' ' ' I ' ' ' ' I ' I ' ri 1-1 • I I . I I , I I ' ' ' ' I ' ' ' u m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #21985: Cyclobutane, 1,i-dimethyl-2-octyl- 5(6 31.40 31.60 31.80 32.00 m/z 55.00 29.64% 5000

* 27 ‘ ' I f' ' ' I '' ' I ' ' ' ' I ' ' ‘ ' I 'I ' ' I ' ' ■' I ' ■m- Ti/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

I

23125.D NP091101.M, Tue Oct 09 12:43:46 2001 Page 6

NYC-WTC_000088035

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NYC-WTC_000088035Source: NYC Law Department, mirrored locally

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