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GC/MS analysis report for sample AD22494, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22494 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086852–000086871

Folder label: “508 Scan 9/15/01 9/26/01

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Scanned page image, NYC-WTC_000086854
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2501\22494.D Vial: 5 Acq On : 25 Sep 2001 6:21 pm Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 Oxirane, 2,3-bis(1-methylethyl Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T.

29.54 4.15 ug/1 472577 Chrysene-dl2 33.15

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, 2,3-bis(1-methylethyl) -, t 128 C8H16O 054644-32-5 32 '2, Cyclobutane, 1, l-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 3 B^yl hexadecanoate 312 C2 0H40O2 000000-00-0 25 4 iZ 3^^ttQxanediol, 2-ethyl-____________ 146 C8H18O2 000094-96-2 23 Abundance Scan 2669 (29,540 min): 22494.D (-) m/z 56.00 rocr;w% T sis

5000 4' 73 ^29 239 312 29.20 29.40 29.60 29.80 T-+-r m/z 57.00 47.11% ■nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane. 2,3-bis(1-methylethyl)-, trans- 53 41

T 29.20 29.40 29.60 29.80 73 m/z 43705 35.78% 113128 J- -r-TT-p-r-r- I'''' I'''' I''''I *''' I JTTT-rp-rTTJ

■nfe-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #21985: Cyclobutane, 1,1 -dimethyl-2-octyl- 55

29.20 29.40 29.60 29.80 A 5000 in/z 41705 33.14%

Ti/z-> A I ' ' ' ' I ' ' 20 40 T k ^1^ 111125140 I • ' I • 60 80 168 196 • r| I . 1 . I I I . I I I .-|-|-|-| I r-r| I I rrj ri ■ ■ । । . ■ ■ j > < > < । ■ < ■ > । > ■ । ■ । • ■ । । j 100 120 140 160 180 200 220 240 260 280 300 Abundance #44549: Butyl hexadecanoate 53 29.20 29.40 29.60 29.80 m/z 73700^ 28.18%

5000 258

240 312 129 I I 1571711^ 214 . . 11 . . II . . 'i r J , . I . I . i' I . .. I . . I 11. . . . I r ' T' ' ' T I ■ I ' ' in 1 ~i iTt-| 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

22494.D NP091101.M Wed Sep 26 15:26:41 2001 Page 1 NYC-WtcLoOOO^M

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NYC-WTC_000086854Source: NYC Law Department, mirrored locally

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