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GC/MS analysis results for sample AD22655, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22655 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087326–000087348

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087338
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22655.D Vial: 14 Acq On : 29 Sep 2001 1:11 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS7 5K.L ********************************************************************* Peak Number 6 Oxirane, 2,3-bis(1-methylethyl Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T.

29.54 0.95 ug/1 138294 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 Oxirane, -bis(1-methylethyl)t 128 C8H16O 054644-32-5 32 2 Cyclobu^ none, 3,3-dimethyl- 98 C6H10O 001192-33-2 27 3 1-He: 6/ 2-methyl- 98 C7H14 006094-02-6 27 4 CycX’t’Utane, 1,1-dimethyl-2-octyl- 196 C14H28 062338-30-1 27 Abundance '■ Scan 2669 (29.544 min); 22655.D (-)' m/z 56.0.0 100.00% 5)6

5000 41 73 257 . 129 239 I . JI,4, .^‘?3l5717l185iQg213 312 29.20 29.40 29.60 29.80 m/z 57.0.0 46.73% Ti/2-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #5067: Oxirane, 2,3-bis(1-methylethyl)-,trans- 5S 41

5000 29.20 29.40 29.60 29.80

m/z-> Abundance 20 JJx 40 60 80 113128 I ' ' ' ’ I ' ' • ' I'' ■ ‘ I'''' I'''' I'''' I 100 120 140 160 180 200 220 240 260 280 300 #^275: Cyclobutanone, 3.3-d:methyl- I ’' ‘ ‘ I m/z 41.0,5 32.99%

56 41 29.20 29.40 29.60 29.80 5000 m/z 43.05 32.93%

...... m/2-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance #63261:1-Hexene. 2-methyl- 5)6 29.20 29.40 29.60 29.80 m/z 73.00 29.23% 41 5000 27 70 98 . Ill ' I'''' I'' I I'''' I' p ' '' I I ‘' I'''' I' ‘' I'''' I . ........... B..... A,,„ 'n/Z“> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 29.20 29.40 29.60 29.80

22655.D NP091101.M Wed Oct 10 14:46:16 2001 Page 6

NYC-WTC_000087338

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NYC-WTC_000087338Source: NYC Law Department, mirrored locally

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