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GC/MS analysis results for sample AD22655, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22655 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087326–000087348

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22655.D Vial: 14 Acq On : 29 Sep 2001 1:11 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★★ Peak Number 7 Butyl tetradecanoate (myristat Concentration Rank 5

R.T. EstConc Area Relative to ISTD R.T.

31.67 0.74 ug/1 108089 Chrysene-dl2 33.16

Hit# of 5 Tentative ID MW MolForm CAS# Qual

(jLjButyl tetradecanoate (myristate) 284 C18H36O2 000000-00-0 86 2^Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 35 3 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 037910-65-9 35 4 Oxirane, 2,3-bis(1-methylethyl) -, t 128 C8H16O 054644-32-5 32 Abundance ’ Scan 2901 (31.674 min): 22655.D (-) “■m/z 56.00 100.00%

5000 4 73 129 J..1II li ,11 I . .149 171T. ...207 241 T 340 31.40 31.60 31.80 32.00 fTWrfTVT¥fT-rVfyTH4yrTTTpT-VTJTHTT-p-rTTJTTT-rfTTTTp+TT^^ m/z 57.00 , 44.63% ni/z-> 20 40 60__ 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance W0186: Butyl tetradecanoate (myristate) 53

5000 229 31.40 31.60 31.80 32.00 73 129 IOC 211 m/z 43.00 , 39.09%

m/z-> I'''' I' 20 40 60 .. y u . . ? . U , 80 100 120 140 160 180 200 220 240 260 280 300 320 340 284 I ft

Abundance #5212; Cyclopentanecarboxylic acid, z-aintpo-, trans- 58

31.40 31.60 31.80 32.00

A 5000 m/ Z 41-0.5 29.34%

30 . 100 129 . I I I I q I I r . I . . . ■ I ■ I . I I' ' '' I m/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #5218; Cyclopentanecarboxylic acid, 2-amino-, cis- 5|B 31.40 31.60 31.80 32.00 m/z 72.95 26.45% 5000

30 ,1 , .??■ .. ......................... •n/z~> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31.40 31.60 31.80 32.00

22655.D NP091101.M Wed Oct 10 14:46:20 2001 Page 7

NYC-WTC_000087339

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