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GC/MS analysis results for sample AD22579, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22579 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087180–000087201

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087192
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22579.D Vial; 7 Acq On ; 28 Sep 2001 6:18 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 6 Butyl tetradecanoate (myristat Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 31.68 0.97 ug/1 160126 Chrysene-dl2 33.17 Hit# Tentative ID MW MolForm CAS# Qual 1 Butyytetradecanoate (myristate) ! 284 C18H36O2! 000000-00-0 72 2 Octa^ecanoic acid, butyl ester 340 C22H44O2! 000123-95-5 64 3 Cyc/opropane, 1-(1-methylethyl)-2-n 210 C15H30 041977-39-3 22 4 Cy/lopentanone, 2,2,5,5-tetramethy'l 140 C9H16O 004541-35-9 22 ^bundan/e Scan 2902 (31.679 min): 22579.D (-) m/z 55.95 100.00% 55 (1

5000 4 73 I 129 285 T 340 31,40 31,60 31,80 32,00 mTz sYTOO 49.06% mZz-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 Abundance #40186: Butyl tetradecanoate (myristate) 5

5000 229 31,40 31,60 31,80 32,00 in/z 43; 05 38.06%

Ti/z-> 40 ' ' I f 111 ■ 11 . . . 1. 111 I,,. 1111 .11 ,.,, I ,,. . I, ,, 11 r., 1, 11. 11 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 ..4........... flibundance '#73570; Octadecanoic acid, butyl ester 55 J 31,40 31,60 31.80 32,00 5000 m/ Z 41.05 X 35.71% 285 340 129 267 185

n/z-> 40 60 I 80 100 120 140 160 180 200 220 240 260 280 300 320 340 241 I I '' f

Sundance #25482: Cyclopropane, 1-(1-methylethyl)-2-nonyl- 55 31.40 31.60 31.80 32.00 m/z 73.00 31721% 5000

42 t 1. •125 182 210 ■n/z-> 40 60 80 100 120 140 160 180 200 220 240 260 280 300 320 340 31,40 31,60 31,80 32,00

22579.D NP091101.M Tue Oct 02 11:50:14 2001 Page 6

NYC-WTC_000087192

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