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GC/MS analysis results for sample AD22579, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22579 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087180–000087201

Folder label: “GC/MS Scan 9/19/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2801\22579.D Vial: 7 Acq On : 28 Sep 2001 6:18 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 5 Cyclopentanecarboxylic acid, 2 Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 29.54 0.94 ug/1 155434 Chrysene-dl2 33.17 Hit# of Tentative ID MW MolForm CAS# Qual 1 Cyclope^tanecarboxylic acid, 2-amin 129 C6H11NO2 : 037910-65-9 35 2 Cyclopentanecarboxylic acid, 2-amin 129 C6H11NO2 040482-05-1 35 3 ButylZ hexadecanoate 312 C20H40O2 000000-00-0 32 4 Undecane, 5-methylene-______________ 168 C12H24 005698-48-6 27 Abundance / Scan 2669 (29.540 min): 22579.D (-) m/z 56.00 100.00% 55

5000 4 73 257 ' ' I ' ' 07 129 239 29.20 29.40 29.60 29.80 312 nrh-r in/z 57.00 43744% ■n/z-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 ^bundance #5218: Cyclopentanecarboxylic acid, 2-ainino-, cis- 55

5000 _^a20_2a4g_ja60_2a80___ m/z 4^700 36.70% 30 129 ,1 . , I '''' I'''' I'''' I'''' I'''' I'''' I'''' I'''' I'''' I'''' I TiZz-> 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 Abundance 55 #5212: Cyclopentanecarboxylic acid, 2-amino-, trans-

Ua, 29.20 29.40 :29.6CI 29.80 5000 m/z 41.05 31.99%

30 129 J _| _______ I • • 111'' ’ ’ I ’' " I'' ’ ■ I' " ' I • " ' I'''' I n/z-> Abundance 20 40 60 80 100 120 140 160 180 200 220 240 260 280 300 #44549: Butyl hexadecanoate JIAaVv ' ' I ' ' ' ' I ' SlB _292g_2a40_ja6gL29:80^_ m/z 55.00 27.86% 5000 258

nZz-> 20 40 60 u 73

■P I 129 i 1571711Q5 214 I '''' I 80 100 120 140 160 180 200 220 240 260 280 300 240 312

29,20 29,40 29,60 29.80

22579.D NP091101.M Tue Oct 02 11:50:12 2001 Page 5

NYC-WTC_000087191

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NYC-WTC_000087191Source: NYC Law Department, mirrored locally

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