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GC/MS analysis results for sample AD22579, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD22579 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087180–000087201

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087190
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\l\DATA\SEP2801\22579.D Vial: 7 Acq On : 28 Sep 2001 6:18 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T, 11.65 0.56 ug/1 79039 1,4-Dichlorobenzene-d4 11.79 Hit# of Tentative ID MW MolForm CAS# Qual

1 1,4-ljichlorobenzene-d4 150 C6C12D4 003855-82-1 42 2 Ben^ne-1,2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 33 3 2-^thyl-6-nitroaniline 152 C7H8N2O2 000570-24-1 12 4 Bet zaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 ^bund^ce Scan 720 (11.648 min): 22579.D (-) m/z 150.00 100470% 1!10

5000 115 52 ” 11.40 11.60 11.80 12.00 444.^14^ 4^ ■nZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 m/z 151.90r ''' I 63.10% Abundance #9593:1,4-Dichlorobenzene-d4 I'iO

5000 115 78 11.40 11.60 11.80 12.00 52 m/z 114 .'90 36710% 87 n/z-> 20 30 35 40 50 T-p-n-q-T 60 70 ‘ I ' ' '' I ' 80 90 44 100 110 120 130 140 150 160 Abundance #9592; Benzene-1,2,3,4-d4-. 5,6-dichloro- 150

115 11.40 11.60 11.80 12.00 5000 52 78 m/z 77495 20.07%

87

mZz-> 20 30 35 I 40 50 ’ I' ' ' ' I ' 60 70 I ' I '' ' ' I' 80 90 4L 100 110 120 130 140 150 160 Abundance #66883; 2-Methyl-6-nitroaniline I T 77 152 11.40 11.60 11.80 12.00 m/z 52.00 13.66%

5000 106 52

tVz-> 20 30

30 40 ' 50 ' '' I ' ' ' ' I ' ' 60 70 80 90 122 135 ............I'■■fl'............... 100 110 120 130 140 150 160 L 11.40 11,60 11,80 12.00

22579.D NP091101.M Tue Oct 02 11:50:10 2001 Page 4

NYC-WTC_000087190

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NYC-WTC_000087190Source: NYC Law Department, mirrored locally

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