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GCMS analysis results for sample AD24488, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24488 conducted on November 13, 2001, identifying unknown compounds.

NYC-WTC_000068585–000068597

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\NOV0501\24488.D Vial: 6 Acq On : 5 Nov 2001 4:50 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 1,4-Dichlorobenzene-d4 Concentration Rank 3

R.T. EstConc Area Relative to ISTD R.T. 11.58 0.54 ug/1 92328 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 1,4-Dichlor)2ibenzene-d4 150 C6C12D4 003855-82-1 72 2 Benzene-l,z2,3,4-d4-, 5,6-dichloro- 150 C6C12D4 002199-69-1 16 3 2-Methy1/6-nitroaniline 152 C7H8N2O2! 000570-24-1 10 4 Benzaldehyde, 2-hydroxy-3-methoxy- 152 C8H8O3 000148-53-8 10 Abundance Scan 712 (11.578 min): 24488,D (-) m/z 149.90 100.00% 1$0

5000 115 ... 52 78 38 44 I, , 11 20 11.40 11.60 11.80 12.00 66 ,1 ®7 ..............''I'" m/z 151.90 61.99% 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9593:1,4-Dichlorobenzene-d4 150

5000 115 78 11 20 11.40 11.60 11 80 12.00 52 m/z 114.90 33793% 35 t''P"'P'"r 4^ n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 150 160 Abundance #9592: Benzene-1,2,3,4-d4-, 5,6-dichloro- liiO ' ' I ' 115 11 20 11.40 11.60 11.80 12.00 5000 52 78 in/z 78.05 . 16.48%

35 87

nfe-> 20 30 I 40 50 60 70 I ' ‘ 80 I' 90 T A T 100 110 120 130 140 150 160 Abundance #66883:2-MethyI-6-nitroaniiine 1' ■ • ' I 77 152 11 20 11.40 11.60 11.80 12.00 m/z 52.00 13.25%

5000 106 ft 52 30 94

ii/z-> 20 Ui30 40 50 60 70 80 90 100 110 120 130 140 150 160 ' I ' ' ' ' I ' ' ' M ' ' ' I ' 11,20 11.40 11.60 11.80 12.00

24488.D NP103001.M Fri Nov 09 12:11:18 2001 Page 4

NYC-WTC_000068596

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NYC-WTC_000068596Source: NYC Law Department, mirrored locally

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