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GCMS analysis results for sample AD24488, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24488 conducted on November 13, 2001, identifying unknown compounds.

NYC-WTC_000068585–000068597

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOVO 501\24488.D Vial; 6 Acq On 5 Nov 2001 4:50 pm Operator: 209 GALOS Sample gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.69 1.66 ug/1 286912 1,4-Dichlorobenzene-d4 11.72

Hit# of 5 'entative ID MW MolForm CAS# Qual

1 2-Penta; me, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 39 2 Morpho ne. 4-methyl- 101 C5H11N0 000109-02-4 9 3 Aceti7 acid. 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 9 4 Ace me 58 C3H6O 000067-64-1 7 Abundance Scan 289 (7.695 min): 24488.D (-) m/z 43.05 100.00% 4)3

5000 59

101 7.40 7.60 7.80 __________ ............................3q I 50 , IL... 71 83 -y-TT-T—ryn-n-T-T—p—r-r-TY^ ' I ' ''I ' I ' ' ' ' I ' ' ' ' I ‘ ' I ' ' ' ' I ' ' ' ' I m/z 59.05 / 47.69% ■n/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3245: 2-Pentanone, 4-hydroxy-4-methyl- 413 •------

5000 59 _V4q__7,6o__7;8o__ago___ :.............. :........... 31 RT 101 .................................... I I 73 7___ . I ' I ' ' ' ' I ' ' ' ' I ' ' ' I I ' ' ' ' I TiZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- 4|3

7.40 7.60 7.80 8.00 5000 16.01% 101 15 71 ,Hi...........! ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I Tlfe-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1-dimethylethyl ester 4(3 ' ' ' ' 7.40 7.60 7.80 8.00 m/z 41.05 8.49%

5000 57

101 15 27 ' I ' ' '' ‘ I ' ‘ ' I ' ' I ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I 7.^ ' 7.60 ' ' 7.^ ' ' 8.00 ■nfe-> 20 30 40 50 60 70 80 90 100 110

24488.D NP103001.M Fri Nov 09 12:11:16 2001 Page 3

NYC-WTC_000068595

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NYC-WTC_000068595Source: NYC Law Department, mirrored locally

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