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GCMS analysis results for sample AD24490, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24490 conducted on November 13, 2001, identifying unknown compounds.

NYC-WTC_000068610–000068621

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C;\HPCHEM\1\DATA\NOV0501\24490.D Vial: 14 Acq On 6 Nov 2001 12:39 am Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method ; C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library ; C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.70 1.07 ug/1 176677 1,4-Dichlorobenzene-d4 11.72 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 40 2 Acetic acid , 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 Morphi ne, 4-methyl- 101 C5H11NO 000109-02-4 9 4 1,3-yDioxolane-2-methanol, 2,4-dimet 132 C6H12O3 053951-43-2 9 Abundance Scan 289 (7.695 min): 24490.D (-) m/z 42.95 100.00% 4)3

5000 59

101 ===T==f-T==p=f=r-i-|=^^ 7.40 7.60 7.80 8.00

JLL ) 69 83 48.96% ■| I I , I I I I I , , T I I ' ' ' ' I ' ' ' ' I ‘ ' I ' ' ' ' I ' ' ' ' I ■m/z 59.05 m/z-> 10 20 30 40 50 I60 70 80 90 100 110 Abundance #64274: 2-Pentanone, 4-hydroxy-4-methyl- 4)3

5000 59 7.40 7.^ 7.^ ' m/z 100.95 21.02%

L 27 101 I 1 83 I I n-+ ' I ' ' ' ' I ' • ‘ ‘ I ’ I ' mZz-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292; Acetic acid. 1,1-dimethylethyl ester 4)3

7.40 7.60 7.80 8.TO 5000 57 m/z 58.05 15.17% 101

T —I i r— —— 15—I I—I— —27 T-Li rLi—1 — I —I I ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ‘ I ' ' ' ' I mfe-> 10 20 30 40 50 60 70 80 9O^1PO 110 Abundance #1640: Morpholine, 4-methyl- ............. ' ' ' I ' ' ‘ ' I ' ' ' ' I ' ' ' ' 4)3 7.40 7.60 7.80 8.00 m/z 41.05 7.10%

5000 101 15 71 I ‘ I ' I 27 ' I I i) ' ' I ' ' 56i ' I ' ' ' ' I ' ' I ' ' ‘ ‘ I ' ' ' ' I ‘ ‘ ' I nn/z-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00

24490.D NP103001.M Fri Nov 09 12:24:31 2001 Page 2

NYC-WTC_000068619

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NYC-WTC_000068619Source: NYC Law Department, mirrored locally

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