Laboratory report documenting GC/MS analysis of sample AD25260 conducted on November 28, 2001.
NYC-WTC_000069452–000069462Folder label: “GCMS Scan X 10/23/01 An 11/9/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report
Data File : C:\HPCHEM\1\DATA\NOV0901\25260.D Vial: 10 Acq On : 9 Nov 2001 9:13 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C;\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T.
7.69 2.81 ug/1 468409 1,4-Dichlorobenzene-d4 11.71
Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Pentanone, -hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Acetic acid,, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 Acetone / 58 C3H6O 000067-64-1 10 4 Morpholine', 4-methyl- 101 C5H11NO 000109-02-4 9 Sundance Scan 288 (7.686 min): 25260.D (-) m/z 42795 100.00% 413
59 5000
101 7.40 7.60 7.80 8.00 83 I ' ' ' ' I ' ' ' ' I ' I ' ' ' I I ' ' ' ' I m/z syToT 51.92% n/z-> 10 20 30 40 50 60 70 80 90 100 110
JL Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 4)3
5000 59 7.40 7.60 7.80 8.00 m/z 101.05 21.08% 15 31 101 I, 1^ I 83 ' I ' '' I I I ' ' ' ' I ' ' ' ' i ''' ' ' I ' Ti/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid. 1,1-dimethylethyl ester 4)3 ' I ‘ ' I ' ' __740_7;6g__7;80_8tg^_ aSB 57 m/z 58.05 17754% 101 27 ' I ' ' ' ' I ' I TTfe-> 10 20 30 40 50 60 70 80^ 90 100^110 Abundance #62322: Acetone 4)3 __Y4O_^,6g_7,80__8t0L_ m/z 41.05 8.19%
58 27 ■I . , I . ' I ' ' ' ' 1 ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I m/z-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00
25260.D NP103001.M Tue Nov 27 12:27:54 2001 Page 2
NYC-WTC_000069461
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NYC-WTC_000069463
Laboratory report documenting GCMS analysis of sample AD25261 conducted on November 28, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069484
Laboratory report documenting GCMS analysis of sample AD25263 conducted on November 28, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069676
Laboratory report documenting GCMS analysis of sample AD25462 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069918
Laboratory report documenting GCMS analysis of sample AD25737 conducted on November 29, 2001, noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069863
Laboratory report documenting GCMS analysis of sample AD25732 conducted on November 29, 2001, noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069697
Laboratory report documenting GCMS analysis of sample AD25495 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069907
Laboratory report documenting GCMS analysis of sample AD25736 conducted on November 29, 2001, noting other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000070054
DEP laboratory report documenting GC/MS results for sample AD25737 analyzed on November 29, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000070143
DEP laboratory report documenting GC/MS results for sample AD25841 analyzed on December 6, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069409
Laboratory report documenting GC/MS analysis of sample AD25073 conducted on November 28, 2001.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069767
Gas chromatography-mass spectrometry analytical results for sample AD25601 analyzed on November 28, 2001, identifying other unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000030752
Laboratory report documenting GCMS analysis of sample AD25940 conducted on December 12, 2001, including surrogate compound data.
1 shared topics · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗Similar subjects in other documents. Similarity does not establish the same event, measurement or conclusion.
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NYC-WTC_000069345
Department of Environmental Protection GCMS scan log entry dated October 23, 2001.
Filed in the same folder
NYC-WTC_000069346
Log sheet recording liquid-liquid extraction parameters and sample processing details for November 2001.
Filed in the same folder
NYC-WTC_000069349
Calibration data for GC/MS analysis including naphthalene and phenanthrene standards dated November 8, 2001.
Filed in the same folder
NYC-WTC_000069357
Laboratory report documenting GC/MS analysis of sample AD25049 conducted on November 28, 2001.
Filed in the same folder
NYC-WTC_000069369
Gas chromatography-mass spectrometry analysis report for sample AD25050 identifying other unknown compounds with violation notation.
Filed in the same folder