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GC/MS analysis results for sample AD25260, Nov 28 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD25260 conducted on November 28, 2001.

NYC-WTC_000069452–000069462

Folder label: “GCMS Scan X 10/23/01 An 11/9/01

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Scanned page image, NYC-WTC_000069460
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\NOV0 901\25260.D Vial: 10 Acq On 9 Nov 2001 9:13 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.44 0.41 ug/1 68117 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 T^tative ID MW MolForm CAS# Qual

1 2-Hexanone / 100 C6H12O 000591-78-6 91 2 2-Hexanony; 4-hydroxy-5-methyl-3-pr 172 C10H20O21 061141-74-0 64 3 2-Hexanqhe, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 4 Methyl /Isobutyl Ketone 10 0 C6H12O 000108-10-1 58 Abundance Scan 152 (6.438 min): 25260.D (-) Tm/z 42795 100.00% 43

58 5000

71 85 100 6.00 6.20 6.40 6.60 6.80

Wz-> 7™.^ 20 30 40 49 50 60 70 .,,.1 I..,,,,,,.,... . ,-r 80 90 100 110 120 130 140 m/z 58705 64732% Abundance #1556: 2-Hexanone 43

58 P I ■ . . I b I C, / I I , . I , I . , -y, , . 5000 6.00 6.20 6.40 6.60 6.80 7n7z 57.00 19.29% 27 71 85 100 I I ................................ Tlfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #15807: 2-Hexanone, 4-hydroxy-5-methyl-3-propyl- 4b

6.00 6.20 6.40 6.60 6.80 5000 m/z 41.05 15.29% 58 27 72 ' I‘ ' ' ' I' ' '' II ' I ' ,1 I ' ' ' ' I'l ' ' ' I ' ' I ' ' ' ' I ' ' ' ' I' '' ' r ' ' ' I ' ' ' ‘ I ' ti/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Sundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43 6.00 6.20 6.40 6.60 6.80 m/z 100.05 10.67% 58 29

■nfe-> ' I ' ' ' ' I ' ' '' I I' ''I ' 20 30 40 50 J, 7 60 70 80 90 100 110 120 130 140 140 6.00 6.20 6.40 6.60 6.80

25260.D NP103001.M Tue Nov 27 12:27:52 2001 Page 1

NYC-WTC_000069460

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NYC-WTC_000069460Source: NYC Law Department, mirrored locally

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