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GCMS analysis results for sample AD24730, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24730 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068893–000068906

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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Scanned page image, NYC-WTC_000068902
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24730.D Vial: 20 Acq On : 6 Nov 2001 6:29 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.43 0.85 ug/1 154973 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 intative ID MW MolForm CAS# Qual 1 2-Hexarj0he 100 C6H12O 000591-78-6 91 2 2-Hexdnone, 4-hydroxy-5-methyl-3-pr 172 C10H20O2i 061141-74-0 74 3 2^>Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 4-i^ethyl Isobutyl Ketone 100 C6H12O 000108-10-1 58 Abundance Scan 151 (6.431 min): 24730.D (-) m/z 42795 100.00% 43

58 5000

100 6.00 6.20 6.40 6.60 6.80 51 Wp I, V ■"Tp-r-r-rYtT'T'TyTrTT-p ? “mTz 58.05 53.93% nZz-> 20 30 40 50 60 70 80 90 iroi101201M140 Abundance #1556; 2-Hexanone 43

58 5000 6.00 6.20 6,40 6.60 6.80 “m/z 41.05 16.13% 27 71 85 IM ........ I .1, , p,,1, , I ,,,, II , nZz-> 20 30 40 70 80 90 100 110 120 130 140 Abundance #15807:2-Hexanone. 4-hydroxy-5-methyl-3-propyl- 4b 6.00 6.20 6.40 6.60 6.80 5000 “mTz 57.00 16.12% 58 27

' I ' ' ' ' I ' ' ' ‘ I I I ? . y...... T)Zz-> 20 30 40 50 60 70 'ro " "90 ioo" i 10 " i:a w' "uo Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43 6.66' 6.^' 6.^' 'e.ro m/z 100.00:11.66% 58 5000 29

71 85 y ' I ' ' ‘ ‘ I ■ • > > I I ■ ■ ■ I ■ 11,' 1 ‘ ‘ I ' ' ' ' 1 ‘ ‘ ‘ I ‘ ‘ ' I ' ' ' ' I ‘ ‘ ‘ I' ' ' ' I' 140 6^0 Tlfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.CX) 6.20 6.40 6.60

24730.D NP103001.M Tue Nov 13 12:11:21 2001 Page 2

NYC-WTC_000068902

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NYC-WTC_000068902Source: NYC Law Department, mirrored locally

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