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GCMS analysis results for sample AD24730, Nov 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GCMS analysis of sample AD24730 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068893–000068906

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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Scanned page image, NYC-WTC_000068903
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24730.D Vial: 20 Acq On : 6 Nov 2001 6:29 am Operator: 209 GALOS Sample : gc/ms unknown Inst ; GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DAT2kBASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanol, 4-methyl- Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.68 0.52 ug/1 95427 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentrative ID MW MolForm CAS# Qual 1 2-Pentang36 4-methyl- 102 C6H14O 000108-11-2 78 2 2-Hexan01 102 C6H14O 000626-93-7 78 3 2-Butanol, 3-methyl- 88 C5H12O 000598-75-4 53 4 2-H^tanol, (S) -________________ 116 C7H16O 006033-23-4 50 Abundance Scan 178 (6.679 min): 2473O.D(-) m/z 45.05 100.00% 3

5CXX)

-r-r-r-ry-T 69 55 I 87 gg 6.40 6.60 6.80 7.00 lii.rnr.|h-ii|i..i|ilil]iiii|i...|i.ll|ilii|ii.i|.iii|rii.|...i| m/z 69.10 16.16% TiZz-> 10 15 20 25 30 35 40 45 50 55 60 65 70 7^ K) 85 90 95 100105 Abundance #63546:2-Pentanol. 4-methyl- 4

5000 6.40 6.60 6.80 7.00 27 m/z 41.05 13.68%

Tife-> Abundance ....I..........ill 10 15 202530^404550556065 70 7580^ 90 95 100105 57 T*+-r X #63584:2-Hexanol 4)5

6.40 6.60 6.80 7.00 5000 m/z 43.00 10.27%

69 |liil|lli®illl|lhl|tiiiprTTi|illl 56 I 87 -nyrmy tnfe-> 10 15 20253035404550556065 70 75 80859095 100105 Abundance 32:2-Butanol,3-methyl- -rTr-.-X7T-ri-.-iT. 45 6.40 6.60 6.80 7.00 m/F 44.05 9.99%

5000

nfe-> 39 I . .4-n... I... S 55

10 15 202530^ 40 45 50 55 60 65 70 75 80 85 90 95 100105 73 i"*’r‘“I”"! •11 Xo 6.60 6.80 7.00

24730.D NP103001.M Tue Nov 13 12:11:32 2001 Page 3

NYC-WTC_000068903

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NYC-WTC_000068903Source: NYC Law Department, mirrored locally

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