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GC/MS analysis report, sample AD23720, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23720 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089218–000089233

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089227
OCR text

OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT1501\23720.D Vial: 16 Acq On : 16 Oct 2001 2:51 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanol, 4-methyl- Concentration Rank 6 R.T. EstConc Area Relative to ISTD R.T. 6.74 0.49 ug/1 46484 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 lentative ID MW MolFdrm. CAS# Qual 1 2-Pentaiu^, 4-methyl- 102 C6H14b . 000108-11-2 83 2 2-Hexandl 102 C6H14O 000626-93-7 83 3 Butan^ 2-ethoxy- 102 C6H14O 002679-87-0 50 4 2-Pq^tanol, 3-methyl- 102 C6H14O 000565-60-6 40 Wsundance Scan 185 (6.742 min): 23720.D (-) m/z 45705 10^700% . 4)5

69

Tife-> 39 II + 56 X. 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 87 l"il|'l"l m/z 6.40 6.60 41.05 6.80 7.00 18.65% Abundance #63547; 2-Pentanol, 4-methyl- 4)5

5000 JJ 6.40 6.60 6,80 7.00 27 m/z 69.00 16.89% 69 I" " r'" I" " I " " I" " I" " I " I" "I'' 'II I" " I" " I" ‘ h3/ 38 'I' ‘" I" " I" " r ‘" I" " r' "I..Y ' I" I' ‘" I" " I" " I'"' I' Tl/Z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 Abundance #63584:2-Hexanol 4

' ' 6.40 -M- 6.60 6.80 7-.00 5000 m/z 43.95 12.77%

Abundance 56 69 I 87 *iTfp-.n 1111.11111111-| 111 ITi |T7ri iTh 1111.11H HI

10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 #63540: Butane, 2-ethoxy- 415____________ _ ---- 640—6.60 -6.80 1 -m/-z-^4'3v05=^12-r35% 7,00 -

73 5000

27 59 .... Ih|I..,|.......Il m 11111.11111 [ 11.. 111. i I H '111 , 87 11111111111 rr 102 11111111111111 . i"m-" ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I tt/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105110 6.60 6.80 7.00

23720.D NP091101.M Tue Oct 16 15:15:46 2001 . Page.2

NYC-WTC_000089227

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NYC-WTC_000089227Source: NYC Law Department, mirrored locally

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