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GC/MS analysis report, sample AD23720, Oct 2001

Machine-extracted title · confidence 100%

Laboratory record for sample AD23720 showing detection of unknown compounds on October 17, 2001.

NYC-WTC_000089218–000089233

Folder label: “GC/MS Scan 9/28/01

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Scanned page image, NYC-WTC_000089228
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OCR status: ok · source: pdftotext

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\1\DATA\OCT1501\23720 .D Vial: 16 Acq On : 16 Oct 2001 2:51 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD R.T. 7.75 1.73 ug/1 162402 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Teiltative ID MW MolForm: CAS# Quail 1 2-Pentanon^ 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 Acetic a d, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 33 3 3-HydroX -2-pentanone 102 C5H10O2 003142-66-3 9 4 Propane, 2-methyl-2-(1-methylethoxy 116 C7H16O 017348-59-3 9 Abundance Scan 295 (7.752 min): 23720.D (-) m/z 42.95 100.00% 4(3

59 5000

101 I' 740 7.60 7.80 8.00 53 . 83 I ' ' ' ' I ' ' ' ' I ''' ' ' I ' ' ' N ' ' ' ' I m/z 59.05 51.24% Tife-> 10 20 30 40 50 60 70 80 90 100 110

L Abundance #64275; 2-Pentanone. 4-hydroxy-4-methyl- 4b

5000- 59 740 7.60 7.80 8.00 m/z 100.95 21.28% 15 31 101

■n/z-> '. 10 I, I I ' I ' ' ' ' I ' 20 30 40 ' ' ■ I ' ''I 50 II60............ 70 ............ 80 90 I.....110 100 ^bundance #3292: Acetic acid. 1.1-dimethylethyl ester 4)3—------ -- ------ -- I ' ' / ' I 7.40 7.60 7.80 8.00 5000 57 m/z 58.05 18.03% 101 15 27 ■ I ' ' .......... ■ .IL. ■ I Tl/Z->______ W 20 30 40 50 60 70 80 90 100 110 ^bundance #1691; 3-Hydroxy-2-pentanone I ■ ■ ' ■ I ' .3|1_ ________ 59__________ r-:--7;40-^' 7.60 ' 7:80 -8.00--- m/z — -4rr0'5‘ 7v82%

5000 45___

Tlfe-> r I I I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' 10 20 30 40 50 I, 60 70 . I 80 , ,,,, ^9^-,, 90 100 110 >.40' '7.60 7.80 8.00

23720.D NP091101.M Tue Oct 16 15:15:48 2001 Page 3

NYC-WTC_000089228

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NYC-WTC_000089228Source: NYC Law Department, mirrored locally

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