Laboratory report documenting GCMS analysis of sample AD24492 conducted on November 13, 2001, identifying unknown compounds.
NYC-WTC_000068634–000068646Folder label: “508 Scan X 10/16/01 A 11/5/01”
OCR status: ok · source: pdftotext
NYC 9/11 Public Portal Document
Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24492.D Vial: 8 Acq On : 5 Nov 2001 6:48 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P
Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 3 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1 R.T. EstConc Area Relative to ISTD R.T. 7.70 1.11 ug/1 200046 1,4-Dichlorobenzene-d4 11.71
Hit# of 5 T^tative ID MW MolForm CAS# Qual
1 2-Pentano^, 4-hydroxy-4-methy 1- 116 C6H12O2 000123-42-2 50 2 MorpholJ^, 4-methyl- 101 C5H11NO 000109-02-4 9 3 3-Hydri -2-pentanone 102 C5H10O2 003142-66-3 9 4 Acetjz^ acid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 9 Abundance Scan 289 (7.698 min): 24492.D {-) m/z 43.00 100.00% 40
59 5000
101 7.40 '7.60' 7.80 8.00 53, 3§l 69 8? m/z I ' ' ' ' I ' ' ' ' I ' ' ' ' I !■' '-I '-''I'l'l ' • ■ I I I ■ ' ' I ’ 59.05 54.34% ■n^-> 10 20 30 40 50 60 70 ' 80 ' ' '90' 100 110 Abundance #3245: 2-Pentanone, 4-hydroxy-4-methyl- 40
5000 59 ' ' 7.40 ' 7.^ ' 7.80 ' ‘ 8.00
-.u m/z 100.95 22.84% 31 r-[-t-i-r-r-r-r-ruJ--p m 101 .................................... I I, 73 , .1 ' I ' ' ' ' I ' ' ' ' I ' ' ' I I ' ' ' ' I ' Ti/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #1640: Morpholine, 4-methyl- 4|3
7.40 7.60 7.80 8.00 5000 in/z 58.05 18.23% 101 15 71 I ?. I 56 I ' ' 1 ' ' I ' I ' ' ‘ ' I'l ' ' ' I ' ' ' ' I ' ' ' ' I ' ' ' ' I ' Ti/z-> 10 20 30 40 50 6070 80 90 100 110 Abundance #1691; 3-Hydroxy-2-pentanone ' I ' ' ' ' I ' ' I ' ' ' ' 31 59 7.40 7.60 7.80 8.00 m/z 40.95 7.21%
5000 45 15 I I ' ' ' ' I ' ' ' ' I ' ' I '' '' I ' || 66 73 84 102
■nfe-> 10 20 30 40 50 60 70 80 90 100 110 7.40 7.60 7.80 8.00
24492.D NP103001.M Fri Nov 09 12:19:54 2001 Page 3
NYC-WTC_000068644
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NYC-WTC_000068572
Laboratory report documenting GCMS analysis of sample AD24487 conducted on November 13, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068585
Laboratory report documenting GCMS analysis of sample AD24488 conducted on November 13, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068447
Laboratory report documenting GCMS analysis of sample AD24473 conducted on November 9, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068659
Laboratory report documenting GCMS analysis of sample AD24640 with detection of unknown compounds on November 13, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068598
Laboratory report documenting GCMS analysis of sample AD24489 conducted on November 13, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068696
Laboratory report documenting GCMS analysis of sample AD24694 with detection of unknown compounds on November 13, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068954
Laboratory report documenting GCMS analysis of sample A024874 identifying unknown compounds on November 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068622
Laboratory report documenting GCMS analysis of sample AD24491 conducted on November 13, 2001, identifying unknown compounds.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068684
Laboratory report documenting GCMS analysis of sample AD24642 with detection of unknown compounds on November 13, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068825
Laboratory report documenting GCMS analysis of sample AD24697 with detection of unknown compounds on November 19, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000068647
Laboratory report documenting GCMS analysis of sample AD24493 with detection of unknown compounds on November 13, 2001.
1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗NYC-WTC_000069601
Laboratory report documenting GCMS analysis of sample AD25457 conducted on November 26, 2001, noting unknown compounds.
1 shared topics · Same agency, volume and box · similarity 0.999
machine-extracted · confidence unavailable · Check page ↗No available related records indexed in this group.
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Log sheet recording liquid-liquid extraction parameters and sample processing details for November 2001.
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Calibration data table for GC/MS instrument used in TCLP analysis, generated on November 5, 2001.
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Laboratory report documenting GCMS analysis of sample AD24487 conducted on November 13, 2001, identifying unknown compounds.
Filed in the same folder
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Laboratory report documenting GCMS analysis of sample AD24488 conducted on November 13, 2001, identifying unknown compounds.
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