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GCMS analysis results for sample AD24492, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24492 conducted on November 13, 2001, identifying unknown compounds.

NYC-WTC_000068634–000068646

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24492.D Vial: 8 Acq On : 5 Nov 2001 6:48 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanol Concentration Rank 4

R.T. EstConc Area Relative to ISTD R.T. 6.67 0.40 ug/1 72868 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hex^ol 102 C6H14O 000626-93-7 83 2 2-H^nol, (R) - 102 C6H14O 026549-24-6 64 3 2-P^tanol, 4-methyl- 102 C6H14O 000108-11-2 64 4 2/Hexanol, (S) - 102 C6H14O 052019-78-0 56 'Xbund^nce Scan 177 (6.670 min); 24492.D (-) m/z 44795 100.00% 4)5

5000

69 39 I h 55 I 87 gg 6,40 6,60 6,80 7.00 h..................... I..... n,lillll|H,,|,,7|7,........... I..... ..................................... mTz 69710^ 20.08% 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #63584: 2-Hexanol 4(5

I I . I y. , . , I r ■ ■ . I . . , , I ’l , , ,

_640__a6g__6,80__7W^_ 69 Wz 43.00 15767% ......................... . 5,6 I , 87 Tp-rTTj-h-rrp-rrrp-rTl-p-rTTpT-rTpTT-|-p4Trp^

Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1794: 2-Hexanol. (R)- 4)5

_a4o__6;6q__a8o__Lpg^_ 5000 m/z 41.05 10.90%

69 55 I 87 " I" “ I'"' I'" H ' I" " I" " I'''' I"'' I''" I"'' I''' n/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63547; 2-Pentanol, 4-methyl- 4|5 6.40 6.60 6.80 7.00 m/z 44.00 9.70%

5000

27 57 f .p„,pl....... ?^|.lll I'" 11" 1111" 11." I". 11" ■ ■ I" " I ■ 87 Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.40 6.60 6.80 7.00

24492.D NP103001.M Fri Nov 09 12:19:52 2001 Page 2

NYC-WTC_000068643

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NYC-WTC_000068643Source: NYC Law Department, mirrored locally

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