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GC/MS analysis results for sample AD22656, Oct 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of sample AD22656 conducted on October 11, 2001, identifying unknown compounds.

NYC-WTC_000087349–000087362

Folder label: “GC/MS Scan 9/19/01

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Scanned page image, NYC-WTC_000087360
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\l\DATA\SEP2801\22656.D Vial: 15 Acq On : 29 Sep 2001 2:10 am Operator:'209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 4 2-Hexanol Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T. 6.74 0.52 ug/1 66915 1,4-Dichlorobenzene-d4 11.78 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanol 102 C6H14O 000626-93-7 83 2 2-Pentanjefl, 4-methyl- 102 C6H14O 000108-11-2 64 3 2-Hex^4iol, (S) - 102 C6H14O 052019-78-0 64 4 2-H^nol, (R) - 102 C6H140 026549-24-6 64 C\bundan^ Scan 185 (6.743 min); 22656.D (-) m7z 44.95 100.00%

5000

41 69 ' ' I ' ' ' ' I ‘ ‘ I ‘ ' I ' ' ' ' I 5356 I 8487 6.40 6.60 6.80 7.00 irr.lllll! +rrTp-rtTi4+TTpTTrp*T+t^^ I'''' I'''' I'''' I'''' I m/z 69.00 16.50% tt/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63584; 2-Hexanol 4b

5000 6xo_a6o_a8o_^to___ mZz 41.05 14.98% 69 19 27,31 4^1 8487 ............ . Tife-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #63546; 2-Pentanol, 4-methyl- 4b 6.40 6.60 6.80 7.00 5000 m/z 43.00 13.39%

27 69 57 42 8487 19 T+p+rry I • 1" I ’ I tt+'-r m/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1769; 2-Hexanol, (S)- 4^ 6.40 6.60 6.80 7.00 m/z 43.95 10.78%

5000

...................”....... 55 8487 I '■ ' ' I r '•I<”'I tt/z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

22656.D NP091101.M Fri Oct 05 10:25:40 2001 Page 4

NYC-WTC_000087360

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NYC-WTC_000087360Source: NYC Law Department, mirrored locally

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