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GC/MS analysis report for sample AD22546, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22546 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086949–000086971

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\l\DATA\SEP2501\22546.D vial: 12 Acq On : 26 Sep 2001 1:14 am Operator: 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params*. LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanol Concentration Rank 13 R.T. EstConc Area Relative to ISTD R.T. 6.75 0.41 ug/1 55666 1,4-Dichlorobenzene-d4 11.79 Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexano, 102 C6H14O 000626-93-7 83 2 2-Peni 6ol, 4-methy1- 102 C6H14O 000108-11-2 78 3 2-Hex;^nol, (R) - 102 C6H14O 026549-24-6 64 4 2-Hexanol, (S) - 102 C6H14O 052019-78-0 64 ^bundfWlce Scan 186 (6.748 min): 22546.D (-) Wz 44.95 100.00%

5000

I* 41 69 6.40 6.60 6.80 7.00 53 56 I 8487 I'''' I''' ‘ I'''' I'' ‘' I I " ' I " " 111111" '' I' " 11" " I" " I' 111111111111111 m/z 69.00 14.32% Ti/z-> Abundance 10 15 20 25 30 35 40 45 50 55 60 65 #63584:2-Hexanol 70 75 80 85 90 95 (1 4b

A________ _______________________ h 5000 , . I . I . I I'f V I I I . I . I I __a4p__a6o__a8o__Aoo^__ “m/z 41.05 13.46% 69 19 2/31 4^1 56 Tl/Z-> Abundance 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 #63547: 2-Pentanol, 4-methyl- jhj -p 6.40 6.60 6.80 7.00 5000- m/z 43.05 10.90%

27 ? 8487 Ti/z-> 10 15 20 25 X30 35 pTT-q44TT]-rrTTpT-r4ynTTyrTTTyr^^ 40 45 50 55 60 65 70 75 80 85 90 95 Abundance #1794: 2-Hexanol, (R)- 4b 640 6.60 6.80 7.00 m/z 44.00 9.21%

5000

69 ..... ..... |"|....................................... 55 84 87 ' I'''' I'''' I'''' I Tl/Z-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 6.40 6.60 6.80 7.00

22546.D NP091101.M Wed Oct 03 14:44:26 2001 Page 2

' NYC-WtC_00'0086958

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NYC-WTC_000086958Source: NYC Law Department, mirrored locally

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