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GC/MS analysis report for sample AD22546, September 2001

Machine-extracted title · confidence 95%

Laboratory results for sample AD22546 indicating other unknown compounds detected via GC/MS on September 27, 2001.

NYC-WTC_000086949–000086971

Folder label: “508 Scan 9/17/01 9/26/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C;\HPCHEM\l\DATA\SEP2501\22546.D Vial: 12 Acq On : 26 Sep 2001 1:14 am Operator; 209 GALOS Sample : GC/MS unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params; LSCINT.P

Quant Method : C;\HPCHEM\1\METHODS\NP091101 .M (RTE Integrator) Title ; 209 625/TCLP calibration table 7/16/01 Library ; C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 9 R.T. EstConc Area Relative to ISTD R.T. 6.51 0.75 ug/1 101494 1,4-Dichlorobenzene-d4 11.79 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hex, me 100 C6H12O 000591-78-6 91 2 OxL me, 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 72 3 exanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 [ethyl Isobutyl Ketone 100 C6H12O 000108-10-1 58 Abundance Scan 160 (6.509 min): 22546.D (-) m/z 42.95 100.00% 43

58 5000

71 85 100 6.20 6.40' ' 6.60 6.80 ' . ^I|. 50 . I , ' I ' ''I I ' m/z 58.05 60.28% Tl/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1556: 2-Hexanone 43

58 5000 _a2g__a40_6,60_a80__ m/z 57.00 18.10% 27 71 85 100 I I •nZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1530: Oxirane. 2-methyl-2-(1-methylethyl)- 43 58 520 ' ' ^40 ' ' 6^ 5000 "mTz 41.05 17.02% 71

30 85 100 ' I ' ' ' 'I' ' ' ' I I '1 ' ' ' ' I ' .1, I ........ ... ... I . -n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone, 4-hydroxy-3-propyl- 43 6.20 6.40 6.60 6.80 m/z 100.05 11.14% 58 5000 29

71 85 100

Ti/z-> . ........ I' 20 30 40 50 60 70 I 80 90 4- ............. . 140 100 110 120 130 140 6.20 6.80

22546.D NP091101.M Wed Oct 03 14:44:24 2001 Page 1 NYC-WTC_000086957

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NYC-WTC_000086957Source: NYC Law Department, mirrored locally

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