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GCMS analysis results for sample AD24493, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24493 with detection of unknown compounds on November 13, 2001.

NYC-WTC_000068647–000068658

Folder label: “508 Scan X 10/16/01 A 11/5/01

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Scanned page image, NYC-WTC_000068655
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File C:\HPCHEM\1\DATA\NOV0501\24493.D Vial: 3 Acq On 5 Nov 2001 1:13 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 6.42 0.65 ug/1 105192 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone 100 C6H12O 000591-78-6 91 2 Oxirane -methyl-2- (1-methylethyl) 100 C6H12O 072221-03-5 72 3 Methyl^ Isobutyl Ketone 100 C6H12O 000108-10-1 64 4 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 56 Abundance Scan 150 (6.423 min): 24493.D (-) m/z 4^705 100.00% 4)3

58 5000

71 85 100 6.00 6.20 6.40 6.60 6.80

nZz-> .. I. 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 p m7z 58.05 60.66% Abundance #63387:2-Hexanone 43

58 5000 6.00 6.20 6.40 6.60 6.80 oc 100 Wz 57.00 17.23% 71 85 Y7rTJTTTTpTTTprTTpTTTyrTTT-r^

m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1530: Oxirane, 2-tnethyl-2-(1-methylethyl)- 4b 58 6.00 6.20 6.40 6.60 6.80 5000 m/z 41.05 15.03% 71

30 66 85 100 ......... . "' I" “ I" " I" " I" " I" " h'" I" " I' mfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63350: Methyl Isobutyl Ketone 4|3 6.00 6.20 6.40 6.60 6.80 m/z 100.00 13.28% 5000 58

27 85 IM 67 T , , _ , , ........ pPr +t p vfz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60 6.80

24493.D NP103001.M Fri Nov 09 12:15:31 2001 Page 1

NYC-WTC_000068655

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NYC-WTC_000068655Source: NYC Law Department, mirrored locally

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