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GC/MS analysis results for sample AD23081, Oct 2001

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Laboratory report documenting GC/MS analysis of sample AD23081 conducted on October 10, 2001, identifying unknown compounds.

NYC-WTC_000087842–000087862

Folder label: “GC/MS Scan 9/21/01

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Scanned page image, NYC-WTC_000087849
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File C:\HPCHEM\1\DATA\OCT0301\23081.D Vial: 8 Acq On 3 Oct 2001 7:29 pm Operator: 209 GALOS Sample gc/ms unknown Inst : GC/MS 209 Mise ■ Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 8

R.T. EstConc Area Relative to ISTD R.T.

6.49 0.65 ug/1 81151 1,4-Dichlorobenzene-d4 11.79

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 7 100 C6H12O 000591-78-6 91 2 Oxirane, <methyl-2-(1-methylethyl) 100C6H12O 072221-03-5 64 3 2-Hexane e, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 4 ^®thy: Isobutyl Ketone 100 C6H12O 000108-10-1 58 Abundance Scan 158 (6.488 min): 23081 .D (-) m/z 42.95 100.00% 4)3

58 5000

71 85 100 6.20 6.40 6.60 6.80 ‘'IO-,,-... I|l| m/z 58.0,5 55.30% m/z~> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1556: 2-Hexanone 40

58 - ' 5000 6.20 6.40 6.60 6.80 m/z 57.00 16.64% 27 85 100 I I , i, 71 ' I ' I m/z~> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1530: Oxirane. 2-rnethyi-2-(1-rnethylethyl)- 43 58 6.20 6.40 6.60 6.80 5000 m/zz 41.05 15.44% 71 30 ; ' p' ................. 85 100 ' I ' ' ‘ 'I' ' ' ' I I ' r-p-TT- Ti/z-> 20 30__ 40 __ 50 60 70 80 90 100 110 120 130 140 Abundance #11968: 2-Hexanone’ 4-hydroxy-3-propyr 43 __J:20__640_Jti^^ 58 m/z 84.95 9.64% 5000 29

'I '' ‘ 'I ' ' ' ' I I ,1 ' I' '' ' I ' 71 85 jyp 140 'n/z-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.20 6.40 6.60 6.80

23081.D NP091101.M Tue Oct 09 10:04:56 2001 Page 1

NYC-WTC_000087849

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