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GCMS analysis results, sample AD23913, Oct 2001

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DEP lab report for GCMS analysis of sample AD23913 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067601–000067618

Folder label: “GCMS Scan X 10/2/01 An 10/17/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\23913.D vial: 6 Acq On : 18 Oct 2001 9:05 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.49 0.8^ ug/1 80333 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanone 100 C6H12O 000591-78-6 91 2 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 83 3 Oxirai , 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 59 4 Methy Isobutyl Ketone 100 C6H12O 000108-10-1 52 Abundance j Scan 158 (6.489 min): 23913.D (-) m/z 42.95 100.00% 43

58 5000

100 6.^ 'e.^' '6.6o' 6.80 85

n/z-> 20 30 40 » ,1,60 70 80 90 100 110 120 130 140 71I I m/z 58.05 52.50% Abundance #1556:2-Hexanone 43

58 5000 I r. . I 6.20 6.40 6.60 6.80 m/z sYToo 16.41% 27 71I 85 100 I 1

nZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968:2-Hexanone, 4-hydroxy-3-propyl- 43 58 6.40 6.60 6.80 5000 29 m/z 41.0.0 16.02%

' I'''' I ‘'''ll ,1 T-p-rV 71 I T*" 86 ryTr-rVnrp-TTT-fT-TTT-TT-rT-T^^ 140 'T»/z-> 20 30 40 50 60 70 80 90 100 110 120 130 w Abundance #1530: Oxirane. 2-methyl-2-(1-methytethyl)- 43 6.20 6.40 6,60 6.80 58 m/z 100.05 12737% 5000 71 30 85 100 A ‘ I''' ‘ I'''' H 20 30 40 50 a)'' ' 'sb' " w imiioiIoimTJo^ 1 ’ ' ’ ' I ’ ‘ ' 'e.^' 6.40 ' I ‘ * 6.60 6.80

23913.D NP101901.M Tue Oct 23 14:34:35 2001 Page 1

NYC-WTC_000067615

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NYC-WTC_000067615Source: NYC Law Department, mirrored locally

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