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GCMS analysis results for sample AD24487, Nov 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24487 conducted on November 13, 2001, identifying unknown compounds.

NYC-WTC_000068572–000068584

Folder label: “508 Scan X 10/16/01 A 11/5/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\NOV0501\24487.D Vial; 5 Acq On : 5 Nov 2001 3:51 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.42 0.69 ug/1 113452 1,4-Dichlorobenzene-d4 11.71

Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanon^ 100 C6H12O 000591-78-6 91 2 Oxirane, >2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 64 3 Methyl Tsobutyl Ketone 100 C6H12O 000108-10-1 58 4 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 50 Abundance Scan 150 (6.419 min): 24487.D (-) m/ z 42.95 100.00% 4|3

58 5000

I' ' ' ' f ' * ‘ ' I ' ‘ 71 85 1M 6.00 6.20 6.40 6.60 6.80 111' 11111111111111111111111" 1111111 m/^ 57.9,5 57.98% Tlfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556:2-Hexanone 43

58 5000 —rr-r-i-TT-rn-r 6.00 6.20 6.40 6.60 6.80 m/z 41.05 16.05% 27 71 85 ... . ....... 'I m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1530: Oxirane. 2-methyl-2-(1-methylethyl)- 4)3 58 6.00 6.20 6.40 6.60 6.80 5000 m/z 57.00 14.54% 71

30 66 85 100 "l"H|.Hl|llll|llll|ll 1111 < I I > 11 I 11111 . rj-i III11111 I .................. I nT/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63354: Methyl Isobutyl Ketone 4)3 6.00 6.20 6.40 6.60 6.80 m/z 100.05 10.73% fflwl 58 85 100

m^-> Jr . II. K 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 111111111111111111111111111111111111

6.00 6.20 6.40 6.60 6.80

24487.D NP103001.M Fri Nov 09 12:00:37 2001 Page 1

NYC-WTC_000068580

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NYC-WTC_000068580Source: NYC Law Department, mirrored locally

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