GCMS analysis results for sample AD26131, Dec 2001

NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\DEC0401 26131.D vial: 70 Acq On : 4 Dec 2001 12:23 pm Operator: 209 GALOS Sample : 11/2 gc/ms Inst : GC/MS 209 Mise t Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP112601.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 3 R.T. EstConc Area Relative to ISTD R.T.

6.42 0.40 ug/1 102002 1,4-Dichlorobenzene-d4 11.70

Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexanone 100 C6H120 000591-78-6 86 2 Oxirane, 2-methyl-2- (1-methylethyl) 100 C6H120 072221-03-5 59 3 Methyl Isobutyl Ketone 100 C6H120 000108-10-1 52 4 2-Hexanone,/4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 39 Abundance Scan 149 (6.415 min): 26131.D (-) m/z 42.95 100.00% 43

58 5000

1/8/8 I i j I i t : । : TTT 18.B TBI T »

. 1 36 । I, 53 71 । | 85 100 6.00 6.20 6.40 6.60 6.80 111 p i 11] > T > 1111 > 111 > > 111 i 11 rn TTHIT m/z 58.05 51.79% m/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63384: 2-Hexanone 43

5000 58 — .... D TR • 6.00 6.20 6.40 6.60 6.80 29 m/z 41.05 17.89% I t | 71 85 190 mz-> Abundance Tmmmmmpppmmmmgmnpp 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #1530: Oxirane, 2-methyl-2-(1-methylethyl)- 43 58 NuN. 6.00 6.20 6.40 6.60 6.80 5000 m/z 57.00 15.41%

miz-> Abundance 30 mmmmmHmmmmmmmm1111 52 66 71

20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 #63351: Methyl Isobutyl Ketone 43 85 100

_W —।। । i । , । > i .. । । . , . । , । . i । . i 6.00 6.20 m/z 100 .05 6.40 6.60 6.80 8.67% 5000 58 27 85 100 m mm 4 mm ■ mmmmmmmmmmm miz—> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60 6.80

26131.D NP112601.M Tue Dec 04 16:07:26 2001 Page 1

NYC-WTC_000031011