GC/MS analysis results for sample AD25073, Nov 28 2001

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Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\NOV0901\25073.D Vial: 14 Acq On : 10 Nov 2001 1:05 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.43 0.41 ug/1 57485 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexanoiie 100 C6H12O 000591-78-6 72 2 Oxiran^ 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 59 3 Methyy Isobutyl Ketone 100 C6H12O 000108-10-1 47 4 2-Hepcanamine, 2-methyl- 129 C8H19N 027581-29-9 38 Abundance Scan 151 (6.427 min): 25073.D (-) m/z 42.95 100700% 40 58 5000

85 100 6.00 6.20 6.40 6.60 6.80

nZz-> 5 J rr rrp-i-rTp-rrrj- 71 7+* 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ,0^ m/z 58.05 63.98% Abundance #63387: 2-Hexanone 40 58 5000 6.00 6.20 6.40 6.60 6.80 "mTz 85.0,5 13.66% 71 85 +r T Ti/z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1530: Oxirane. 2-methyl-2-(1-methylethyl)- 40 58 ,I 6.00 6.20 6.40 6.60 6,80 5000 "m/z 99?^ 12.53% 71

66 85 100 4.^ TrrpTTTpTTT|TTITyTTTTp-rTT-|T^^ " " I'"' I" " I" " I" " I" " II nfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Sundance #63353: Methyl Isobutyl Ketone I ' ' ' ' I ' ' 40 6.00 6.20 6.40 6.60 630 m/z 57.00 11.45% 5000 58

27 ■85 100 15 67 pTTTp-rTrlTTTTJTTTTpTT-r^^ p-rr Tl/Z-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.00 6.20 6.40 6.60 6.80

25073.D NP103001.M Tue Nov 27 11:11:56 2001 Page 1

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