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GCMS analysis results for sample AD24873, Nov 2001

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Laboratory report documenting GCMS analysis of sample AD24873 identifying unknown compounds on November 19, 2001.

NYC-WTC_000068942–000068953

Folder label: “GCMS Scan X 10/17/01 An 11/6/01

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Scanned page image, NYC-WTC_000068950
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\NOV0601\24873.D Vial: 2 Acq On : 6 Nov 2001 1:46 pm Operator: 209 GALOS San^le : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params? LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP103001.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C;\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.43 0.58 ug/1 117619 1,4-Dichlorobenzene-d4 11.71 Hit# of 5 tative ID MW MolForm CAS# Qual 1 2-Hexano: 100 C6H12O 000591-78-6 91 2 Oxiranp< 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 64 3 Methyl Isobutyl Ketone 100 C6H12O 000108-10-1 58 4 2-Hexanone, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 56 Scan 151 (6.431 tnin): 24873.D (-) m/z 42.95 100.00% 4^

58 5000

I'''' I'''' I'''' I'' 85 100 6.00 6.20 6.40 6.60 36 I I, . 49 53 I , 71 Tiprrrqiiri । rn , 111 rl j I (-tM m/z 58.05 50.69% 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1556:2-Hexanone 43

58 5000 6.00 6,20 6.40 6.60 6.80 “mTz 41.00 16.32% 27 85 I T»Zz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1530: Oxirane, 2-methyl-2-(1-inelhyl8thyl)- 43 58 6.66 6.^ 6.40 6.TO 6.^ 5000 “m/z 57.00 16.00% 71

30 ............... ..... "I 66 ................Tu,... Tife-> 2)25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63350: Methyl Isobutyl Ketone 43 6.00 6.20 6.40 6.60 6.80 m/z 100.05 11.59% 5000

Tife-> An 27 1 ’ ” ‘ I' ’ " I ’ 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 58

85 1M p-tT-r[TTTTJTTTTYrTTT|TT^^

6^ 1 6.20 6.40 6.60 6.80

24873.D NP103001.M Fri Nov 16 11:52:28 2001 Page 1

NYC-WTC_000068950

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NYC-WTC_000068950Source: NYC Law Department, mirrored locally

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