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GCMS analysis results for sample AD23995, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD23995 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067752–000067766

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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Scanned page image, NYC-WTC_000067761
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NYC 9/11 Public Portal Document

Library Search Compound Report

Data File : C:\HPCHEM\1\DATA\OCT2501\23995.D Vial: 3 Acq On : 25 Oct 2001 2:39 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr; 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.44 1.00 ug/1 157803 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 2-HexanoM 100 C6H12O 000591-78-6 91 2 Methyl ^pbutyl Ketone 100 C6H120 000108-10-1 52 3 Oxi ri , 2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 45 4 Prop: lal 58 C3H6O 000123-38-6 43 Niundance • Scan 152 (6.438 min): 23995.D (-) m/z 42795 100.00%

58 5000

gw gw 6.40 6.60 6.80 53. 1 . 71 ....................... I ‘ ' ■ I' I 'l' " ■ I ■ ■' •! I' ‘ ‘ I • ■ " I ■' ■' I'' ‘ • I ‘‘ I' ■ ’ ■ I' ' ' U ‘‘ I ■m/z 58.05 55.68% +t ■nfe-> 20 25 30 35 40 45 50 55 W 65 70 75 W 85 90 95 100 105 Abundance #1556:2-Hexanone 43

58 5000 gw 6.W 6.40 gw gw ■m/z 57700 15.01% 27 71 85 100 .. . -►t Tlfe-> 20 25 30 35 40 45 W55W65 70 75 W 85 90 95 1W105 Abundance #63354: Methyl isobulyl Ketone 40 6.00 ‘ gw g^ gw gw 5000 41.05 14.28% 58 A I 85 100 rTTTTTTrrTTTTTTnTTTlTUTTTTTTnTTrTriltp^ Tlfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90^ 100105 ^bundance #1530: Oxirane, 2-m8thyI-2-(1-methylethyl)- 4(3 gw_gw_gw_gw_gw_ 58 m/z 100.05 10.28% 5000 71 . 52 I 66 85 100 ■TpT-rTpT-rT|TTrTpTTTyHHTr|TTTTJT4+q444iyrTTTy+TTT]4TTTyTTTTpTTTfrT^^ ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 aw'' 6.20 6.^

23995.D NP101901.M Fri Oct 26 10:08:16 2001 Page 2

NYC-WTC_000067761

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NYC-WTC_000067761Source: NYC Law Department, mirrored locally

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