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GC/MS analysis results for sample AD23344, Oct 19 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23344 conducted on October 19, 2001.

NYC-WTC_000088683–000088694

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088691
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\23344.D Vial: 12 Acq On : 19 Oct 2001 2:57 am Operator: 209 GALOS Sample : gc/ms unknown re extracted Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE 'Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD 'R.T. 6.49 0.5/ ug/1 49617 1,4-Dichlorobenzene-d4 11.76 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 2-Hexai/one 100 C6H12O 000591-78-6 90 2 Oxira:, 2-methyl-2-(1-methylethyl) 100C6H12O 072221-03-5 78 3 Methy Isobutyl Ketone 100 C6H12O 000108-10-1 64 4 Propanal 58 C3H6O 000123-38-6 47 Abundance * m/z Scan 158 (6.489 min): 23344. D (-) 42.95 100.00% 4)3

58 5000

71 85 IW 6.20 6.40 6.60 6.80 53 '' I ‘ ‘' I"" I'"' I"' h + +trrrTTTT+vtr 11' ‘' 11''' I ‘' I'''' I'' ‘' I ‘' 11'' 11'' ‘' I 'i"-r 54.83%

“ Z■ ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #1556: 2-Hexanone 43

58 5000- ^1 " 6.20 6.40 6.60 6.80 m/z 56.95 :17.77% 27 71 85 100 " 1 ■ " 11 ■ I " I" " I" • 11 • I - Ti/2-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 ^bundance #1530: Oxirane, 2-methyl-2-(1 -methylethyl)- 4)3 58 6.20 6.40 6.60 6.80 5000 "mTz 41.05 17.64% 71

30 66 85 100 52 I ■r| [ I I I I 1111 11 -nym-rp- Tp-rI................ Trq-rrrrp- 20 25 30 3^401 45 50 5^0 65/07b&0 85 90 95 100 105 Sundance #63354: Methyl Isobutyl Ketone 43 6.20 6.40 6.60 6.80 . m7z 3^/95 10.83%

5000-

' 11" I' I' 1111' I" I'" 11 + ' I " ' ‘ I " " I' 58 85 100 ' I" ' ‘ I " " I " " I" " I " " I " " I " " I" " I I""I UI nw gj ■n/z-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.20 6.40 6.60 6.80

23344.D NP091101.M Fri Oct 19 10:14:06 2001 Page 1

NYC-WTC_000088691

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NYC-WTC_000088691Source: NYC Law Department, mirrored locally

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