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GC/MS analysis results for sample AD23344, Oct 19 2001

Machine-extracted title · confidence 100%

Laboratory report documenting GC/MS analysis of environmental sample AD23344 conducted on October 19, 2001.

NYC-WTC_000088683–000088694

Folder label: “GC/MS Scan 9/26/01

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Scanned page image, NYC-WTC_000088692
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\23344.D Vial: 12 Acq On : 19 Oct 2001 2:57 am Operator: 2 09 GTkLOS Sample : gc/ms unknown re extracted Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Pentanone, 4-hydroxy-4-methy Concentration Rank 1

R.T. EstConc Area Relative to ISTD ’R.T. 7.76 0.79 ug/1 76769 1,4-Dichlorobenzene-d4 11.76 . Hit# of 5 Tentative ID MW MolForm CAS# Qual

1 2-Pent^one, 4-hydroxy-4-methyl- 116 C6H12O2 000123-42-2 50 2 5-Hexe/-2-one 98 C6H10O 000109-49-9 9 3 Aceti acid, 1,1-dimethylethyl este 116 C6H12O2 000540-88-5 9 4 Morpty line, 4-methyl- 101 C5H11NO 000109-02-4 5 Abundance Scan 296 (7.756 min); 23344.D (-) m/z 42.95 100.00% ft 59 5000

101 _^4g_j,6g__7,8g_aoo__ ' I ' ' ' ' I ' ' ' ' I - m/z 59705 50.48% m/z-> 10 20 30 40 50 60 70 80 90 100 110 Abundance #64275: 2-Pentanone, 4-hydroxy-4-methyl- 4)3

I ___________ 5000- 59 740 7.60 7.80 8.00 m/z 100.95 19.12% 15 31 -l-r-rT-rvj-T- 101

I 83 ' l'" " I I ' I ' ' ' ' I ' ' ' ' I ' m/z~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #63205: 5-Hexen-2-one 4)3

7.40 7^ 7.80 8.00 5000 58.05 17.84%

55 38 , 50 I 83 98 ' I ''' ' ' I ' ' ' ' I ' ' 1 ' I ' ' nfe~> 10 20 30 40 50 60 70 80 90 100 110 Abundance #3292: Acetic acid, 1,1-dimethylethyl ester ■ I 4)3 7.40 7.60 7.80 8.00 m/z 41.05 6.72%

5000 57

1 101

■nfe-> 27 I ' ' ' ' I ' ' ' ' I 10 20 30 40 50 III 60 70 80 90 100 I ; 110 7.40 7.60 7.80 8.00

23344.D NP091101.M Fri Oct 19 10:14:08 2001 Page 2

NYC-WTC_000088692

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NYC-WTC_000088692Source: NYC Law Department, mirrored locally

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