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GC/MS analysis results for sample AD23833, Nov 1 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GC/MS analysis of sample AD23833 conducted on November 1, 2001, identifying unknown compounds.

NYC-WTC_000089461–000089475

Folder label: “GC/MS Scan 10/1/01

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Scanned page image, NYC-WTC_000089470
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NYC 9/11 Public Portal Document

Library Search Compound Report Data File ; C:\HPCHEM\1\DATA\OCT3001\23833.D Vial: 18 Acq On : 31 Oct 2001 7:06 am Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2

R.T. EstConc Area Relative to ISTD R.T. 6.42 0.91 ug/1 125070 1,4-Dichlorobenzene-d4 11.71 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 2-Hexano^ 100 C6H12O 000591-78-6 91 2 Oxirane/2-methyl-2-(1-methylethyl) 100 C6H12O . 072221-03-5 80 3 2-Hexa^ne, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 64 4 Methyl/Isobutyl Ketone ________ 100 C6H12O 000108-10-1 58 Abundance Scan 149 (6.416 min): 23833.D (-) m/z 47795 100.00% 43

58 5000

100 6.00 6,20 6.40 6.60 6.80 , 49 i-rTTT*T^ „ I,.. ^1.77, m/z 58705 58.33% ' I > > ‘ > 1' •'' I'''' 1 ■ ' I ’ ’ ' ' I ' ' ’ ' I ' ' ' ' I ' ' TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 ‘Abundance #63387:2-Hexanone 43

58 5000 6.00 6.20 6.40 6.60 6.80 100 m/z 57.00 18.42% 71 85 ■ I ' I • I I I I I I'l I I I ' I ' ' ' ' I ' ' ' ' I ' TiZz-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #1530: Oxirane. 2-methyl-2-(1-methylethyl)- '43 58 6.00 6.20 77^^ 6.40 6.60 6.80 5000 “m/z 41.00 14.70% 71

_______ __ 30_____ 85__LOO____^_____ I ' ' I ' I ' . I, ,1,; I r-,I".... I... 7,......... nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #11968:2-Hexanone. 4-hydroxy-3-propyl- ■;±=:-r43 "6:00^6.20~~6.40~~6:60~^6:80~ m/ z 100.00 13.32% 58 5000 29

,1, ' I'''' I' 71 85 100 A 7 ' ' ' I ' ' ' ' 1 ' ' ' ' I * ' I ' ■nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 6.00 6.20 6.40 6.60 6.80

23833.D NP103001.M Thu Nov 01 13:18:24 2001 Page 2

’NYC-WTC_OOOO8947O

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NYC-WTC_000089470Source: NYC Law Department, mirrored locally

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