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GCMS analysis results for sample AD24051, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD24051 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067880–000067893

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\24051.D Vial: 12 Acq On : 25 Oct 2001 11:26 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method s C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 2 2-Hexanone Concentration Rank 2 R.T. EstConc Area Relative to ISTD R.T. 6.47 0.92 ug/1 183111 1,4-Dichlorobenzene-d4 11.73 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 2-Hexano: 100 C6H12O 000591-78-6 90 2 Oxirane,/2-methyl-2-(1-methylethyl) 100 C6H12O 072221-03-5 78 3 2-Hexa^ne, 4-hydroxy-3-propyl- 158 C9H18O2 062338-17-4 74 4 Methyy Isobutyl Ketone 100 C6H12O 000108-10-1 58 (Abundance / Scan 155 (6.470 min): 24051 .D (-) m/z 42.95 100.00%! 43

58 553

100 '' 'e.^' 'e.eo' s.so ' 51 n* J. 71 I 85 I in/z 58705 57719% nfe-> 20 30 40 50 60 70 80 90 100 110 120 130 140 Abundance #63386:2-Hexanone 43

553 58 ■ 1'''' I' ■'' 6.20 6,40 6.60 6.80 29 m7z 57.00 17.94%

Tife-> V-Mr 20 30 —40- 50 60 70 80 90 100 110 W 1^ Abundance #1530: Oxirane. 2-methyl-2-(1-methylethyl)- 4)3 58 ..... 'e.^' 6.^' 6.60' 6,80 ' 5000 m/z 41.05 16.18% 71 30 85 100 ■ I • ■ ■ ‘ i ■ • ■ • 11 I ■''' I'' ‘' I' ‘' I ■ Tite-> 20 30 40 60 70 80 90 100 110 120 130 140 Abundance #11968; 2-Hexanone, 4-hydroxy-3-propyl- 43 6.20 6.40 6.60 6.80 58 m/z 100.00 11.65% 5000 29

... ,1 ' ' ' 71' ' " I ' 85 '1 ' I 100 1 I 11 11 I. . ........... w, ■nfe-> 20 30 40 ' sb'" 60 70 80 90 100 110 120 130 140 ' 'e.^' 'e.^' 's.eo' 'e.so '

24051.D NP101901.M Fri Oct 26 10:29:07 2001 Page 2

NYC-WTC_000067889

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NYC-WTC_000067889Source: NYC Law Department, mirrored locally

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