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GCMS analysis results for sample AD23995, Oct 29 2001

Machine-extracted title · confidence 95%

Laboratory report documenting GCMS analysis of sample AD23995 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067752–000067766

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : Cs\HPCHEM\l\DATA\OCT2501\23995.D vial: 3 Acq On : 25 Oct 2001 2:39 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 4 R.T. EstConc Area Relative to ISTD R.T. 6.34 0.51 ug/1 80337 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexanoi^ •100 C6H12O 000589-38-8 86 2 3-Pent^ii^e, 2-methyl- 100 C6H12O 000565-69-5 46 3 Butaji^ 2,2-dimethyl- 86 C6H14 000075-83-2 45 4 H§x^e, 2,4,4-trimethyl-___________ 128 C9H20 016747-30-1 36 Abundance Scan 141 (6.337 min): 23995.D (-) m/z 43.05 100.00% 43 57

71 5000 100

6.00 6.20 6.40 6.60 85 p-m-pT 1““1‘ m/z 57.00 86.86% TiZz-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #1528:3-Hexanone 57

29 71 5000 6.00 6.^ ’ 6.^ 6.60 100 m/z 71.00 55.58% T—- tTTTJTTTrp ■nfe-> 10 15^)25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance

lA #63398:3-Pentanone, 2-rnethyl- 5|7 43 . . I . ?vn I . . I . . , , I, I rI I 6.00 6.20 6.40 6.60 5000 Wz 9979^^ 33.96% 100 71 '............... 38 ................................. 85 < 111111111 > > 11 (11 > > 11H11 ■ I«111 > I i I (n • 11.11111.11-> 1. 1111.11111111. <. 11,.. 1111.1 < I.. { u, IJ, o , I,,,, 11,,, 11 Tlfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #732: Butane. 2,2-ditiiethyl- nA lO , ■ I. ■ f,. I 43 517 6.00 71 m/z 41.00 26.46% 29 5000

15 1 nfe-> 5 10 15 202530354045505560^ 70 7580859095 100105 6.00 6.20 6.40 6.60

23995.D NP101901.M Fri Oct 26 10:08:14 2001 Page 1

NYC-WTC_000067760

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NYC-WTC_000067760Source: NYC Law Department, mirrored locally

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