GCMS analysis results for sample AD23998, Oct 29 2001

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Library Search Compound Report Data File s C:\HPCHEM\1\DATA\OCT2501\23998.D Vial: 6 Acq On : 25 Oct 2001 5:35 pm Operator: 209 GALOS San^le : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.37 0.51 ug/1 105283 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 3-Hexancme 100 C6H12O 000589-38-8 74 2 3-Pent^one, 2-methyl- 100 C6H12O 000565-69-5 50 3 Butan^ 2,2 - dimethyl - 86 C6H14 000075-83-2 45 4 3-Hep^anone, 4-methyl-__________ 128 C8H16O 006137-11-7 42 4bunctence Scan 144 (6.367 min): 23998.D (-) m/z 43.00 100.00% 43 57

71 5000 100

85 6.00 6.20 6.40 6.60 6.80 m/z 57.00 89.34% Tlfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 1001 (» Abundance #63357:3-Hexanone 4(3 57 29 5000 71 6 00 6.^ 6,40 ‘s.SO 6,80 100 m/z 71.00 58.43% .,1.1.111111111.11111L1.11.... __________ _______ L_ I....1.1111... 11.1,11.__ 85 I,,., I,.,, I,,,. I,.,11,,,,I,,,,I. 1,.,, ,I,, 11111., I,,.. nfe-> 5 10 15 20^ 30 35 40 45 50 55 60 6S 70 75 «)85 90 95 100105 Abundance #63398:3-Pentanone, 2-methyl- 5(7 43 ..... 6.00 6.20 5000 m/z 100.05 37.11% 100

LJyu 71 85 I””! n''H|i..,ii tTTTy r nfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance #732: Butane. 2,2-dImethyl- 43 5|7 6,00 6,2) 6.40 6.60 6.80 71 mT^ 41.05 23.75% 29 5000

<5 I I I , I , I . , 11 I . , I ,, ,, I . T 1- ■ I <{ "< i| ' >1 'I

•nfe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 100105 6.00 6.20 6.40 6.60 6.80

23998.D NP101901.M Fri Oct 26 10:12:16 2001 Page 1

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