GC/MS analysis results for sample AD23502, Oct 2001

NYC 9/11 Public Portal Document Library Search Compound Report Data File : 'C:\HPCHEM\1\DATA\OCT1601\23502.D Vial: 10 Acq On : 16 Oct 2001 11:02 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplr: 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NES75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 14 R.T. EstConc Area Relative to ISTD R.T. 6.38 0.45 ug/1 46337 1,4-Dichlorobenzene-d4 11.76 Hit# Of 5 Tentative ID MW MolForm CAS# Qual

1 3-Hex^one 100 .C6H12O 000589-38-8 87 2 3-Pen/anone, 2-methyl- 100 C6H12O 000565-69-5 58 3 2,4-^entanedione 100 C5H8O2 000123-54-6 43 4 Butane, 2,2-dimethyl- 86 C6H14 000075-83-2 42 Abundance Scan 146 (6.384 min): 23502. D (-) m/z 43.00 100.00% 4^ 5|7

71 5000 100

6.00 6.20 6.40 6.60 6.80 85 p m/z 57.00 95.56% 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #63358:3-Hexanone 43 57

71 5000- 6.00 6.20 6.40 6.60 6.60 100 m/z 71.00 6T7T3%

I' " ' I' ’'' I 'T'"I""I' ............ ... ......... " I " " I' nZz-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 '100 105 Abundance #63398: 3-Pentanone, 2-methyl- _______________________ 5(7___ __ ____ 43 6.00 6.20 6.40 6.60 6.80 5000 100 71 38 85 r+ tTT nfe-> ^bundance #63324: 2,4-Pentaneclione 43 6.00 6.20 6.40 6.60 6.80 .m/z_.41.00 28..-21% 5000 85 100

27 38,1 58 _____________________________ 72 Tj n I 11 I I I 11 ■ I 11 iTi +> Jt I I I I I < 111 I i > I I I 11 ■ I I I <> I I I I ,> I I I I 111 I I I 11 I > 11 I I ■ < [ J 11 r 111 I I I 11 p 6.00 6.20 ' 6.40 ' 6.60 6.80 Tlfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105

23502.D NP091101.M Thu Oct 18 10:24:41 2001 Page 1

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