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GCMS analysis results for sample AD24046, Oct 29 2001

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Laboratory report documenting GCMS analysis of sample AD24046 conducted on October 29, 2001, noting unknown compounds.

NYC-WTC_000067811–000067825

Folder label: “GCMS Scan X 10/5/01 An 10/25/01

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT2501\24046.D Vial: 7 Acq On : 25 Oct 2001 6:33 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise Multiplr: 1.00 MS Integration Params: LSCINT.P Quant Method : C:\HPCHEM\1\METHODS\NP101901.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.36 0.49 ug/1 90460 1,4-Dichlorobenzene-d4 11.74 Hit# of 5 Tentative ID MW MolForm CAS# Qual 1 3-Hexa: fne 100 C6H12O 000589-38-8 91 2 3-Buti -2-01 72 C4H8O 000598-32-3 38 3 3-Pe: anone, 2-methyl- 100 C6H12O 000565-69-5 38 4 But e, 2,2-dimethyl -___________ 86 C6H14 000075-83-2 36 Abundance Scan 143 (6.359 min): 24046.D (-) mTz 43.05 100.00% 4{3 57

71 5000 100 AjV/v^. 6.20 6.40 6.60 6.80 86 +nTTT I ra/^ 57.00 90.27% Ttife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 'Abundance #63358:3-Hexanone 43 57

5000 71 6.00 ^40 ' 6.TO ' ‘ 6.^ 100 m/z 71.00 63.47%

LL. 85 ++prrTpTTTT I""I‘ Tife-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 Abundance #62480:3-Buten-2-ol 517 43 6.00 6.20 (6.40 6.60 6.80 5000 m/z 100.0532.51% 27 71 H...... ii|, Jl"l V....... 1‘ ’ 1' ‘ ‘ I Tife::>__^_^_J0^_4g_^_50^_60_^_J0_^_M_K_9g_^_100jira a,bundance #63398:3-Pentanone. 2-methyl- 5t7 600 6.20 6.40 6.60 6.80 43 “m/z 41.00 27771% 5000 100 71 85 l"*’l +1 :• I" " I'"' I' -PTTT p ■nfe-> 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100 105 6.00 6.20 6.40 6.60 6.80

24046.D NP101901.M Fri Oct 26 12:20:22 2001 Page 1 NYC-WTC_000067819

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NYC-WTC_000067819Source: NYC Law Department, mirrored locally

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