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GCMS analysis results, sample AD23909, Oct 2001

Machine-extracted title · confidence 100%

DEP lab report for GCMS analysis of sample AD23909 conducted on October 23, 2001, noting unknown compounds.

NYC-WTC_000067555–000067578

Folder label: “GCMS Scan X 10/2/01 An 10/17/01”

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NYC 9/11 Public Portal Document

Library Search Compound Report Data File : C:\HPCHEM\1\DATA\OCT1801\23909.D vial: 4 Acq On : 18 Oct 2001 7:07 pm Operator: 209 GALOS Sample : gc/ms unknown Inst : GC/MS 209 Mise : Multiplrt 1.00 MS Integration Params: LSCINT.P

Quant Method : C:\HPCHEM\1\METHODS\NP091101.M (RTE Integrator) Title : 209 625/TCLP calibration table 7/16/01 Library : C:\DATABASE\NBS75K.L ********************************************************************* Peak Number 1 3-Hexanone Concentration Rank 5 R.T. EstConc Area Relative to ISTD R.T. 6.38 0.52 ug/1 48449 1,4-Dichlorobenzene-d4 11.77 Hit# of 5 'entative ID MW MolForm CAS# Qual 1 3-Hexan^e 100 C6H12O 000589-38-8 86 2 3-Pent^one, 2-methyl- 100 C6H12O 000565-69-5 47 3 Butane, 2,2-dimethyl- 86 C6H14 000075-83-2 36 4 2,4 'entanedione 100 C5H8O2 000123-54-6 35 Scan 146 (6.379 min): 23909.D (-) m/z 43.05 100.00% 43 57

71 5000 100

6.00 6,20 6.40 6,60 6.80 rrpTTTTTTrry m/z 57700 83.42% TTfe-> 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ^bundance #63358:3-Hexanone 4)3 57

5000 71 6.ro' 'e.^' 6.40 6.OT aro 100 m/z 71.00 56.01% 85 Mr i""i M l""l''ninii|

XIm Tife-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 Abundance t: 3-Pentanone, 2-methyl- 5|7 43 6.(M 6.20 6.^ 6,60 6.TO 5000 m/z 100.05 35.43% 100 71 85 rrTrrrmT T'fe-> 5 10 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 ^bundance #732: Butane, 2,2-dimethyl- .......... 43 5|7 600 6,20 6.40 ' ‘ 6.^ ' SOT 71 m/z 41.00 19.28% 29 5000

IS 11 , ■ I. < I J I 1 ■ ■ I ■ ■ I I 11 T 111 I I I, III I + 1 11 11 I 11 IE I I • 11 11111 11 111 I II , 11 111 11 11.11 111 I I IH I, II I|iII I I II I ,I

Tlfe-> 5 1O 15 20 25 30 35 40 45 50 55 60 65 70 75 80 85 90 95 100105 6.66 " q'w ' 6.80

23909.D NP101901.M Tue Oct 23 14:32:25 2001 Page 1

NYC-WTC_000067572

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NYC-WTC_000067572Source: NYC Law Department, mirrored locally

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GCMS analysis results, sample AD23910, Oct 2001 · Box DEP Box 60

NYC-WTC_000067579

Gas chromatography-mass spectrometry analysis of sample AD23910 conducted by NYC Department of Environmental Protection labs on October 23, 2001, identifying unknown compounds.

1 shared non-person entities · 1 shared topics · Same agency, volume and box · similarity 0.999

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